3-[(1S,2S)-1-((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyl)-3,3,4,4-tetramethyl-1-oxo-1λ⁵-phosphetan-2-yl]-propan-1-ol

Base Information

• Chemical Name: 3-[(1S,2S)-1-((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyl)-3,3,4,4-tetramethyl-1-oxo-1λ⁵-phosphetan-2-yl]-propan-1-ol
• CAS No.: 217467-42-0
• Molecular Formula: C₂₀H₃₉O₂P
• Molecular Weight: 342.502

Synonyms:3-[(1S,2S)-1-((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyl)-3,3,4,4-tetramethyl-1-oxo-1λ⁵-phosphetan-2-yl]-propan-1-ol

Chemical Property of 3-[(1S,2S)-1-((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyl)-3,3,4,4-tetramethyl-1-oxo-1λ⁵-phosphetan-2-yl]-propan-1-ol

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Technology Process of 3-[(1S,2S)-1-((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyl)-3,3,4,4-tetramethyl-1-oxo-1λ⁵-phosphetan-2-yl]-propan-1-ol

There total 1 articles about 3-[(1S,2S)-1-((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyl)-3,3,4,4-tetramethyl-1-oxo-1λ⁵-phosphetan-2-yl]-propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1S,4S)-4-Allyl-1-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-2,2,3,3-tetramethyl-phosphetane 1-oxide (190850-90-9) → 3-[(1S,2S)-1-((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyl)-3,3,4,4-tetramethyl-1-oxo-1λ5-phosphetan-2-yl]-propan-1-ol (217467-42-0)

Guidance literature:

With sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; water; dihydrogen peroxide; Yield given. Multistep reaction; 1.) THF, 25 deg C, 3 h, 2.) r.t., 1 h;

DOI:10.1055/s-1998-2169

Reference yield: 95.0%

3-[(1S,2S)-1-((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyl)-3,3,4,4-tetramethyl-1-oxo-1λ5-phosphetan-2-yl]-propan-1-ol (217467-42-0) → 3-[(1R,2S)-1-((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyl)-3,3,4,4-tetramethyl-phosphetan-2-yl]-propan-1-ol

Guidance literature:

With trichlorosilane; triethylamine; In benzene; at 25 ℃; for 4h;

DOI:10.1055/s-1998-2169

Reference yield:

3-[(1S,2S)-1-((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyl)-3,3,4,4-tetramethyl-1-oxo-1λ5-phosphetan-2-yl]-propan-1-ol (217467-42-0) → (1R,4S)-4-(3-Diphenylphosphanyl-propyl)-1-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-2,2,3,3-tetramethyl-phosphetane

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / Et₃N, Cl₃SiH / benzene / 4 h / 25 °C

With trichlorosilane; triethylamine; In benzene;

DOI:10.1055/s-1998-2169

upstream raw materials:

(1S,4S)-4-Allyl-1-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-2,2,3,3-tetramethyl-phosphetane 1-oxide

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