Technology Process of 4-(amino)cyclooctanone
There total 5 articles about 4-(amino)cyclooctanone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 77 percent / tetramethylammonium periodate / CHCl3 / 17 h / Ambient temperature
2: 91 percent / potassium azodicarboxylate, AcOH / methanol / 5 h / Ambient temperature
3: sodium phosphate, 6percent sodium amalgam / ethanol / 3 h / 0 °C
4: 98 percent / CrO3, H2SO4 / acetone
With
chromium(VI) oxide; sodium amalgam; tetramethylammonium metaperiodate; sulfuric acid; potassium diazodicarboxylate; acetic acid; sodium phosphate;
In
methanol; ethanol; chloroform; acetone;
DOI:10.1016/S0040-4020(01)80257-X
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 77 percent / tetramethylammonium periodate / CHCl3 / 17 h / Ambient temperature
2: 91 percent / potassium azodicarboxylate, AcOH / methanol / 5 h / Ambient temperature
3: sodium phosphate, 6percent sodium amalgam / ethanol / 3 h / 0 °C
4: 98 percent / CrO3, H2SO4 / acetone
With
chromium(VI) oxide; sodium amalgam; tetramethylammonium metaperiodate; sulfuric acid; potassium diazodicarboxylate; acetic acid; sodium phosphate;
In
methanol; ethanol; chloroform; acetone;
DOI:10.1016/S0040-4020(01)80257-X
