16-(cyclohex-1-enylthio)-17,18,19,20-tetranorprostaglandin F_2α methyl ester

Base Information

Chemical Name:16-(cyclohex-1-enylthio)-17,18,19,20-tetranorprostaglandin F_2α methyl ester
CAS No.:59739-49-0
Molecular Formula:C₂₃H₃₆O₅S
Molecular Weight:424.602
Hs Code.:

16-(cyclohex-1-enylthio)-17,18,19,20-tetranorprostaglandin F<sub>2α</sub> methyl ester

Synonyms:16-(cyclohex-1-enylthio)-17,18,19,20-tetranorprostaglandin F_2α methyl ester

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Chemical Property of 16-(cyclohex-1-enylthio)-17,18,19,20-tetranorprostaglandin F_2α methyl ester

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Technology Process of 16-(cyclohex-1-enylthio)-17,18,19,20-tetranorprostaglandin F_2α methyl ester

There total 4 articles about 16-(cyclohex-1-enylthio)-17,18,19,20-tetranorprostaglandin F_2α methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 59739-48-9
16-(cyclohex-1-enylthio)-17,18,19,20-tetranorprostaglandin F_2α 9-acetate methyl ester

: 59739-49-0,73285-92-4
16-(cyclohex-1-enylthio)-17,18,19,20-tetranorprostaglandin F_2α methyl ester

Guidance literature:: With potassium carbonate; In methanol; at 40 - 45 ℃; for 1h;
DOI:10.1021/jm00179a010

Reference yield:

: 60894-66-8
<1α(Z), 2β(1E), 3α, 5α>-7-<5-(acetyloxy)-2-(2-formylethenyl)-3-<(tetrahydro-2H-pyran-2-yl)oxy>cyclopentyl>-5-heptenoic acid methyl ester

: 59739-49-0,73285-92-4
16-(cyclohex-1-enylthio)-17,18,19,20-tetranorprostaglandin F_2α methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-butyllithium / 1.) THF, hexane, 5 deg C, 3 h, 2.) THF, hexane, -78 deg C, 1 h

2: 70 percent / 65percent aq. acetic acid / tetrahydrofuran / 1 h / 40 °C

3: 85 percent / K₂CO₃ / methanol / 1 h / 40 - 45 °C

With n-butyllithium; potassium carbonate; acetic acid; In tetrahydrofuran; methanol;
DOI:10.1021/jm00179a010

Reference yield:

: 4410-13-3
1-(methylthio)cyclohexene

: 59739-49-0,73285-92-4
16-(cyclohex-1-enylthio)-17,18,19,20-tetranorprostaglandin F_2α methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-butyllithium / 1.) THF, hexane, 5 deg C, 3 h, 2.) THF, hexane, -78 deg C, 1 h

2: 70 percent / 65percent aq. acetic acid / tetrahydrofuran / 1 h / 40 °C

3: 85 percent / K₂CO₃ / methanol / 1 h / 40 - 45 °C

With n-butyllithium; potassium carbonate; acetic acid; In tetrahydrofuran; methanol;
DOI:10.1021/jm00179a010