1-(3-chlorophenyl)-6-hydroxy-4-methyl-2-oxo-1,2-dihydropyridine-3-carbonitrile

Base Information

Chemical Name:1-(3-chlorophenyl)-6-hydroxy-4-methyl-2-oxo-1,2-dihydropyridine-3-carbonitrile
CAS No.:944746-56-9
Molecular Formula:C₁₃H₉ClN₂O₂
Molecular Weight:260.68
Hs Code.:

Synonyms:1-(3-chlorophenyl)-6-hydroxy-4-methyl-2-oxo-1,2-dihydropyridine-3-carbonitrile

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Chemical Property of 1-(3-chlorophenyl)-6-hydroxy-4-methyl-2-oxo-1,2-dihydropyridine-3-carbonitrile

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Technology Process of 1-(3-chlorophenyl)-6-hydroxy-4-methyl-2-oxo-1,2-dihydropyridine-3-carbonitrile

There total 1 articles about 1-(3-chlorophenyl)-6-hydroxy-4-methyl-2-oxo-1,2-dihydropyridine-3-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 17722-12-2
N-(3-chlorophenyl)-2-cyanoacetamide

: 141-97-9
ethyl acetoacetate

: 944746-56-9
1-(3-chlorophenyl)-6-hydroxy-4-methyl-2-oxo-1,2-dihydropyridine-3-carbonitrile

Guidance literature:: With potassium hydroxide; for 0.166667h; Equilibrium constant; Microwave irradiation;
DOI:10.1007/s00706-012-0911-5

Reference yield:

: 164656-28-4
C₁₂H₁₄N₂O₂

: 944746-56-9
1-(3-chlorophenyl)-6-hydroxy-4-methyl-2-oxo-1,2-dihydropyridine-3-carbonitrile

: 944746-57-0
C₂₅H₂₀ClN₅O₄

Guidance literature:: C₁₂H₁₄N₂O₂; With nitrosylsulfuric acid; In water; acetic acid; propionic acid; at 0 - 5 ℃; for 1h;

1-(3-chlorophenyl)-6-hydroxy-4-methyl-2-oxo-1,2-dihydropyridine-3-carbonitrile; With sodium carbonate; urea; In water; acetic acid; propionic acid; at 0 - 5 ℃; for 3h;