3-((6-aminoquinazolin-4-yl)amino)-4-(dimethylamino)-N-methylbenzenesulfonamide

Base Information

Chemical Name:3-((6-aminoquinazolin-4-yl)amino)-4-(dimethylamino)-N-methylbenzenesulfonamide
CAS No.:1301761-40-9
Molecular Formula:C₁₇H₂₀N₆O₂S
Molecular Weight:372.451
Hs Code.:

Synonyms:3-((6-aminoquinazolin-4-yl)amino)-4-(dimethylamino)-N-methylbenzenesulfonamide

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Chemical Property of 3-((6-aminoquinazolin-4-yl)amino)-4-(dimethylamino)-N-methylbenzenesulfonamide

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Technology Process of 3-((6-aminoquinazolin-4-yl)amino)-4-(dimethylamino)-N-methylbenzenesulfonamide

There total 2 articles about 3-((6-aminoquinazolin-4-yl)amino)-4-(dimethylamino)-N-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1301761-87-4
4-(dimethylamino)-N-methyl-3-[(6-nitro-4-quinazolinyl)amino]benzenesulfonamide

: 1301761-40-9
3-((6-aminoquinazolin-4-yl)amino)-4-(dimethylamino)-N-methylbenzenesulfonamide

Guidance literature:: With hydrogen; palladium-on-charcoal; In methanol; at 25 ℃; for 2.5h;

Reference yield:

: 19815-16-8
4-chloro-6-nitro-quinazoline

: 1301761-40-9
3-((6-aminoquinazolin-4-yl)amino)-4-(dimethylamino)-N-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: isopropyl alcohol

2: hydrogen; palladium 10% on activated carbon / methanol / 2.5 h / 25 °C

With palladium 10% on activated carbon; hydrogen; In methanol; isopropyl alcohol;
DOI:10.1021/acs.jmedchem.6b01342

Reference yield: 1.4%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1301761-40-9
3-((6-aminoquinazolin-4-yl)amino)-4-(dimethylamino)-N-methylbenzenesulfonamide

: 76-05-1
trifluoroacetic acid

: 4-(dimethylamino)-N-methyl-3-((6-(methylamino)quinazolin-4-yl)amino)benzenesulfonamide bis(trifluoroacetate)

: 4-(dimethylamino)-3-((6-(dimethylamino)quinazolin-4-yl)amino)-N-methylbenzenesulfonamide bis(trifluoroacetate)

Guidance literature:: formaldehyd; 3-((6-aminoquinazolin-4-yl)amino)-4-(dimethylamino)-N-methylbenzenesulfonamide; With sodium tris(acetoxy)borohydride; acetic acid; In dichloromethane; water; at 25 ℃; for 0.0833333h;

With sodium tris(acetoxy)borohydride; In dichloromethane; water; at 25 ℃; for 2h;

trifluoroacetic acid; In water; acetonitrile;