Technology Process of C19H19N3O5
There total 6 articles about C19H19N3O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
water; lithium hydroxide;
In
tetrahydrofuran; methanol;
at 0 ℃;
for 0.5h;
DOI:10.1021/jm100022r
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1.25 h / 0 - 25 °C
2.1: pyridine / 130 °C
3.1: methanol; lithium hydroxide; water / tetrahydrofuran / 2 h
3.2: pH 4
With
pyridine; methanol; lithium hydroxide; oxalyl dichloride; water;
N,N-dimethyl-formamide;
In
tetrahydrofuran; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / dichloromethane; chloroform; water; isopropyl alcohol
1.2: 0.5 h
2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1.25 h / 0 - 25 °C
3.1: pyridine / 130 °C
4.1: methanol; lithium hydroxide; water / tetrahydrofuran / 2 h
4.2: pH 4
With
pyridine; methanol; lithium hydroxide; osmium(VIII) oxide; oxalyl dichloride; water; 4-methylmorpholine N-oxide;
N,N-dimethyl-formamide;
In
tetrahydrofuran; dichloromethane; chloroform; water; isopropyl alcohol;