Technology Process of C21H26N4O3S
There total 5 articles about C21H26N4O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
ammonium molibdate; dihydrogen peroxide;
In
ethanol;
at 0 ℃;
for 21h;
DOI:10.1021/ol1028699
- Guidance literature:
-
Multi-step reaction with 2 steps
1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 4 h / 0 °C
2: ammonium molibdate; dihydrogen peroxide / ethanol / 21 h / 0 °C
With
ammonium molibdate; di-isopropyl azodicarboxylate; dihydrogen peroxide; triphenylphosphine;
In
tetrahydrofuran; ethanol;
1: Mitsunobu reaction;
DOI:10.1021/ol1028699
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere
1.2: 10 h / 0 - 20 °C / Inert atmosphere
2.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 6 h / 0 - 20 °C / Inert atmosphere
3.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere
With
di-isopropyl azodicarboxylate; sodium hydride; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/acs.orglett.9b03857