(2-methyl-5-tert-butylphenyl) 2-O-benzoyl-4,6-di-O-benzyl-1-thio-α-D-mannopyranoside

Base Information

Chemical Name:(2-methyl-5-tert-butylphenyl) 2-O-benzoyl-4,6-di-O-benzyl-1-thio-α-D-mannopyranoside
CAS No.:1361016-64-9
Molecular Formula:C₃₈H₄₂O₆S
Molecular Weight:626.814
Hs Code.:

Synonyms:(2-methyl-5-tert-butylphenyl) 2-O-benzoyl-4,6-di-O-benzyl-1-thio-α-D-mannopyranoside

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Chemical Property of (2-methyl-5-tert-butylphenyl) 2-O-benzoyl-4,6-di-O-benzyl-1-thio-α-D-mannopyranoside

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Technology Process of (2-methyl-5-tert-butylphenyl) 2-O-benzoyl-4,6-di-O-benzyl-1-thio-α-D-mannopyranoside

There total 6 articles about (2-methyl-5-tert-butylphenyl) 2-O-benzoyl-4,6-di-O-benzyl-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: C₃₉H₄₄O₆S

: 1361016-64-9
(2-methyl-5-tert-butylphenyl) 2-O-benzoyl-4,6-di-O-benzyl-1-thio-α-D-mannopyranoside

Guidance literature:: With acetic acid; In tetrahydrofuran; water; at 20 ℃; for 2h;
DOI:10.1016/j.bmc.2011.12.048

Reference yield:

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 1361016-64-9
(2-methyl-5-tert-butylphenyl) 2-O-benzoyl-4,6-di-O-benzyl-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1.1: pyridine; acetic anhydride / 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: pyridine / 0 °C / Inert atmosphere

3.1: N,N-dimethyl-formamide / 0.17 h / 7.5 Torr

3.2: 3 h

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

5.1: sodium hydride / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

6.1: acetic acid / tetrahydrofuran; water / 2 h / 20 °C

With pyridine; tetrabutyl ammonium fluoride; acetic anhydride; sodium hydride; acetic acid; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.12.048

Reference yield:

: 1361016-58-1
(2-methyl-5-tert-butylphenyl) 1-thio-α-D-mannopyranoside

: 1361016-64-9
(2-methyl-5-tert-butylphenyl) 2-O-benzoyl-4,6-di-O-benzyl-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine / 0 °C / Inert atmosphere

2.1: N,N-dimethyl-formamide / 0.17 h / 7.5 Torr

2.2: 3 h

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

5.1: acetic acid / tetrahydrofuran; water / 2 h / 20 °C

With pyridine; tetrabutyl ammonium fluoride; sodium hydride; acetic acid; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.12.048