1-<2-(2'-tetrahydropyranyloxyethyl)thienyl>-2-(methoxymethyloxymethyl)cyclohexaneazido

Base Information

Chemical Name:1-<2-(2'-tetrahydropyranyloxyethyl)thienyl>-2-(methoxymethyloxymethyl)cyclohexaneazido
CAS No.:174316-92-8
Molecular Formula:C₂₀H₃₁N₃O₄S
Molecular Weight:409.55
Hs Code.:

Synonyms:1-<2-(2'-tetrahydropyranyloxyethyl)thienyl>-2-(methoxymethyloxymethyl)cyclohexaneazido

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Chemical Property of 1-<2-(2'-tetrahydropyranyloxyethyl)thienyl>-2-(methoxymethyloxymethyl)cyclohexaneazido

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Technology Process of 1-<2-(2'-tetrahydropyranyloxyethyl)thienyl>-2-(methoxymethyloxymethyl)cyclohexaneazido

There total 2 articles about 1-<2-(2'-tetrahydropyranyloxyethyl)thienyl>-2-(methoxymethyloxymethyl)cyclohexaneazido which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 174316-80-4
1-<2-(2'-tetrahydropyranyloxyethyl)thienyl>-2-(methoxymethyloxymethyl)cyclohexanol

: 174316-81-5
1-<2-(2'-hydroxyethyl)thienyl>-2-(methoxymethyloxymethyl)cyclohexaneazido

: 174316-92-8
1-<2-(2'-tetrahydropyranyloxyethyl)thienyl>-2-(methoxymethyloxymethyl)cyclohexaneazido

Guidance literature:: With sodium azide; Trichlormethylhydroperoxid; In chloroform; at 0 - 20 ℃; for 19h;
DOI:10.1002/(SICI)1099-1344(199601)38:1<77::AID-JLCR815>3.0.CO;2-X

Reference yield:

: 174316-79-1
2-(methoxymethyloxymethyl)cyclohexanone

: 174316-92-8
1-<2-(2'-tetrahydropyranyloxyethyl)thienyl>-2-(methoxymethyloxymethyl)cyclohexaneazido

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) THF, 0 deg C, 30 min, 2.) THF, 15 deg C, 2 h

2: 78 percent / NaN₃, Cl₃COOH / CHCl₃ / 19 h / 0 - 20 °C

With n-butyllithium; sodium azide; Trichlormethylhydroperoxid; In chloroform;
DOI:10.1002/(SICI)1099-1344(199601)38:1<77::AID-JLCR815>3.0.CO;2-X

Reference yield: 44.7%

: 174316-92-8
1-<2-(2'-tetrahydropyranyloxyethyl)thienyl>-2-(methoxymethyloxymethyl)cyclohexaneazido

: (1S,2R)-2-Methoxymethoxymethyl-1-{5-[2-(tetrahydro-pyran-2-yloxy)-ethyl]-thiophen-2-yl}-cyclohexylamine

: (1S,2S)-2-Methoxymethoxymethyl-1-{5-[2-(tetrahydro-pyran-2-yloxy)-ethyl]-thiophen-2-yl}-cyclohexylamine

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 8h; Heating;
DOI:10.1002/(SICI)1099-1344(199601)38:1<77::AID-JLCR815>3.0.CO;2-X