N'-(anthracen-9-ylmethylene)-3,5-bis(3,5-bis(benzyloxy)benzyloxy)benzohydrazide

Base Information

Chemical Name:N'-(anthracen-9-ylmethylene)-3,5-bis(3,5-bis(benzyloxy)benzyloxy)benzohydrazide
CAS No.:1312750-31-4
Molecular Formula:C₆₄H₅₂N₂O₇
Molecular Weight:961.126
Hs Code.:

Synonyms:N'-(anthracen-9-ylmethylene)-3,5-bis(3,5-bis(benzyloxy)benzyloxy)benzohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N'-(anthracen-9-ylmethylene)-3,5-bis(3,5-bis(benzyloxy)benzyloxy)benzohydrazide

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Technology Process of N'-(anthracen-9-ylmethylene)-3,5-bis(3,5-bis(benzyloxy)benzyloxy)benzohydrazide

There total 7 articles about N'-(anthracen-9-ylmethylene)-3,5-bis(3,5-bis(benzyloxy)benzyloxy)benzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1312750-30-3
C₄₉H₄₄N₂O₇

: 642-31-9
9-anthracene aldehyde

: 1312750-31-4
N'-(anthracen-9-ylmethylene)-3,5-bis(3,5-bis(benzyloxy)benzyloxy)benzohydrazide

Guidance literature:: In methanol; chloroform;
DOI:10.1021/ol201325j

Reference yield:

: 137472-14-1
methyl 3,5-bis[[3,5-bis(phenylmethoxy)phenyl]methoxy] benzoate

: 1312750-31-4
N'-(anthracen-9-ylmethylene)-3,5-bis(3,5-bis(benzyloxy)benzyloxy)benzohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / tetrahydrofuran; methanol / 12 h / 70 °C

2: methanol; chloroform

With hydrazine hydrate; In tetrahydrofuran; methanol; chloroform;
DOI:10.1021/ol201325j

Reference yield:

: 2150-44-9
1-carbomethoxy-3,5-dihydroxybenzene

: 1312750-31-4
N'-(anthracen-9-ylmethylene)-3,5-bis(3,5-bis(benzyloxy)benzyloxy)benzohydrazide

Guidance literature:: Multi-step reaction with 6 steps

1: tetra-(n-butyl)ammonium iodide; potassium carbonate / 1,4-dioxane / 24 h / Reflux

2: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / Inert atmosphere; Reflux

3: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C

4: tetra-(n-butyl)ammonium iodide; potassium carbonate / acetone / 24 h / Reflux

5: hydrazine hydrate / tetrahydrofuran; methanol / 12 h / 70 °C

6: methanol; chloroform

With lithium aluminium tetrahydride; thionyl chloride; tetra-(n-butyl)ammonium iodide; potassium carbonate; hydrazine hydrate; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; chloroform; acetone;
DOI:10.1021/ol201325j