(2,2-dimethyl-5,7-dioxo-1,3-dioxocan-6-yl)-(4-iodophenyl)iodonium ylide

Base Information

Chemical Name:(2,2-dimethyl-5,7-dioxo-1,3-dioxocan-6-yl)-(4-iodophenyl)iodonium ylide
CAS No.:1428552-13-9
Molecular Formula:C₁₂H₁₀I₂O₄
Molecular Weight:472.018
Hs Code.:

Synonyms:(2,2-dimethyl-5,7-dioxo-1,3-dioxocan-6-yl)-(4-iodophenyl)iodonium ylide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2,2-dimethyl-5,7-dioxo-1,3-dioxocan-6-yl)-(4-iodophenyl)iodonium ylide

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Technology Process of (2,2-dimethyl-5,7-dioxo-1,3-dioxocan-6-yl)-(4-iodophenyl)iodonium ylide

There total 2 articles about (2,2-dimethyl-5,7-dioxo-1,3-dioxocan-6-yl)-(4-iodophenyl)iodonium ylide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 2033-24-1
cycl-isopropylidene malonate

: 73178-09-3
-p-iodobenzene

: 1428552-13-9
(2,2-dimethyl-5,7-dioxo-1,3-dioxocan-6-yl)-(4-iodophenyl)iodonium ylide

Guidance literature:: With potassium hydroxide; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1016/j.tetlet.2013.02.018

Reference yield: 19.0%

: 2033-24-1
cycl-isopropylidene malonate

: 624-38-4,1032416-46-8
para-diiodobenzene

: 1428552-13-9
(2,2-dimethyl-5,7-dioxo-1,3-dioxocan-6-yl)-(4-iodophenyl)iodonium ylide

Guidance literature:: para-diiodobenzene; With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃;

cycl-isopropylidene malonate; With potassium hydroxide; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1016/j.tetlet.2013.02.018

Reference yield: 70.0%

: 1428552-13-9
(2,2-dimethyl-5,7-dioxo-1,3-dioxocan-6-yl)-(4-iodophenyl)iodonium ylide

: 153750-28-8
1-[¹⁸F]fluoro-4-iodobenzene

Guidance literature:: With tetrabutylammonium bicarbonate; [18F]fluoride ion, cyclotron produced, NCA; In dimethyl sulfoxide; at 110 ℃; Solvent; Temperature;
DOI:10.3390/molecules20010470