(E)-1-(3,5-dimethylphenyl)-2-{4-[(trimethylsilyl)ethynyl]phenyl}diazene

Base Information

Chemical Name:(E)-1-(3,5-dimethylphenyl)-2-{4-[(trimethylsilyl)ethynyl]phenyl}diazene
CAS No.:1253299-33-0
Molecular Formula:C₁₉H₂₂N₂Si
Molecular Weight:306.483
Hs Code.:

Synonyms:(E)-1-(3,5-dimethylphenyl)-2-{4-[(trimethylsilyl)ethynyl]phenyl}diazene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-(3,5-dimethylphenyl)-2-{4-[(trimethylsilyl)ethynyl]phenyl}diazene

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Technology Process of (E)-1-(3,5-dimethylphenyl)-2-{4-[(trimethylsilyl)ethynyl]phenyl}diazene

There total 1 articles about (E)-1-(3,5-dimethylphenyl)-2-{4-[(trimethylsilyl)ethynyl]phenyl}diazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 67083-40-3
1,3-dimethyl-5-nitrosobenzene

: 75867-39-9
4-trimethylsilylethynyl aniline

: 1253299-33-0
(E)-1-(3,5-dimethylphenyl)-2-{4-[(trimethylsilyl)ethynyl]phenyl}diazene

Guidance literature:: With acetic acid; for 14h;
DOI:10.1002/ejoc.201000650

Reference yield: 64.0%

: 1253299-33-0
(E)-1-(3,5-dimethylphenyl)-2-{4-[(trimethylsilyl)ethynyl]phenyl}diazene

: 4,8,12-tri-n-propyl-4,8,12-triaza-triangulenium tetrafluoroborate

: 1227608-99-2
(E)-12c-[4-(3,5-dimethylphenyldiazenyl)phenyl]ethynyl-4,8,12-tri-n-propyl-4,8,12-triazatriangulene

Guidance literature:: (E)-1-(3,5-dimethylphenyl)-2-{4-[(trimethylsilyl)ethynyl]phenyl}diazene; With potassium hydroxide; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere; Sonication;

4,8,12-tri-n-propyl-4,8,12-triaza-triangulenium tetrafluoroborate; In tetrahydrofuran; at 0 ℃; for 5h; Sonication;
DOI:10.1002/ejoc.201000650