2-chloro-6-[(Z)-1(3H)-isobenzofuranylidenemethyl]-9-(methoxyphenylmethyl)-9H-purine

Base Information

Chemical Name:2-chloro-6-[(Z)-1(3H)-isobenzofuranylidenemethyl]-9-(methoxyphenylmethyl)-9H-purine
CAS No.:1192179-34-2
Molecular Formula:C₂₂H₁₇ClN₄O₂
Molecular Weight:404.856
Hs Code.:

Synonyms:2-chloro-6-[(Z)-1(3H)-isobenzofuranylidenemethyl]-9-(methoxyphenylmethyl)-9H-purine

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Chemical Property of 2-chloro-6-[(Z)-1(3H)-isobenzofuranylidenemethyl]-9-(methoxyphenylmethyl)-9H-purine

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Technology Process of 2-chloro-6-[(Z)-1(3H)-isobenzofuranylidenemethyl]-9-(methoxyphenylmethyl)-9H-purine

There total 2 articles about 2-chloro-6-[(Z)-1(3H)-isobenzofuranylidenemethyl]-9-(methoxyphenylmethyl)-9H-purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 10602-08-1
2-ethynylbenzyl alcohol

: 115204-74-5
2,6-dichloro-9-(4-methoxyphenylmethyl)-9H-purine

: 1192179-34-2
2-chloro-6-[(Z)-1(3H)-isobenzofuranylidenemethyl]-9-(methoxyphenylmethyl)-9H-purine

Guidance literature:: 2-ethynylbenzyl alcohol; 2,6-dichloro-9-(4-methoxyphenylmethyl)-9H-purine; With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; In N,N-dimethyl-formamide; at 60 ℃; for 5h; Inert atmosphere;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

With sodium hydrogencarbonate; In dichloromethane; water; Saturated solution;
DOI:10.1016/j.bmc.2009.08.012

Reference yield:

: 10602-08-1
2-ethynylbenzyl alcohol

: 115204-74-5
2,6-dichloro-9-(4-methoxyphenylmethyl)-9H-purine

: 2-chloro-6-[(E)-1(3H)-isobenzofuranylidenemethyl]-9-(methoxyphenylmethyl)-9H-purine

: 1192179-34-2
2-chloro-6-[(Z)-1(3H)-isobenzofuranylidenemethyl]-9-(methoxyphenylmethyl)-9H-purine

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; In N,N-dimethyl-formamide; at 60 ℃; for 5h; optical yield given as %de; Inert atmosphere;
DOI:10.1016/j.bmc.2009.08.012