(E)-N⁴-(2-(diethylamino)ethyl)-N¹-(1-(1-(1-(methoxy(methyl)amino)-4-methyl-1-oxopentan-2-ylamino)-4-methyl-1-oxopentan-2-ylamino)-4-methyl-1-oxopentan-2-yl)-2-(pyrrolidin-1-yldiazenyl)terephthalamide

Base Information

• Chemical Name: (E)-N⁴-(2-(diethylamino)ethyl)-N¹-(1-(1-(1-(methoxy(methyl)amino)-4-methyl-1-oxopentan-2-ylamino)-4-methyl-1-oxopentan-2-ylamino)-4-methyl-1-oxopentan-2-yl)-2-(pyrrolidin-1-yldiazenyl)terephthalamide
• CAS No.: 1013658-00-8
• Molecular Formula: C₃₈H₆₅N₉O₆
• Molecular Weight: 743.991

Synonyms:(E)-N⁴-(2-(diethylamino)ethyl)-N¹-(1-(1-(1-(methoxy(methyl)amino)-4-methyl-1-oxopentan-2-ylamino)-4-methyl-1-oxopentan-2-ylamino)-4-methyl-1-oxopentan-2-yl)-2-(pyrrolidin-1-yldiazenyl)terephthalamide

Chemical Property of (E)-N⁴-(2-(diethylamino)ethyl)-N¹-(1-(1-(1-(methoxy(methyl)amino)-4-methyl-1-oxopentan-2-ylamino)-4-methyl-1-oxopentan-2-ylamino)-4-methyl-1-oxopentan-2-yl)-2-(pyrrolidin-1-yldiazenyl)terephthalamide

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Technology Process of (E)-N⁴-(2-(diethylamino)ethyl)-N¹-(1-(1-(1-(methoxy(methyl)amino)-4-methyl-1-oxopentan-2-ylamino)-4-methyl-1-oxopentan-2-ylamino)-4-methyl-1-oxopentan-2-yl)-2-(pyrrolidin-1-yldiazenyl)terephthalamide

There total 1 articles about (E)-N⁴-(2-(diethylamino)ethyl)-N¹-(1-(1-(1-(methoxy(methyl)amino)-4-methyl-1-oxopentan-2-ylamino)-4-methyl-1-oxopentan-2-ylamino)-4-methyl-1-oxopentan-2-yl)-2-(pyrrolidin-1-yldiazenyl)terephthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

(S)-2-Amino-4-methyl-pentanoic acid {(S)-1-[(S)-1-(methoxy-methyl-carbamoyl)-3-methyl-butylcarbamoyl]-3-methyl-butyl}-amide; compound with trifluoro-acetic acid + lithium (E)-4-(((2-diethylamino)ethyl)carbamoyl)-2-(pyrrolidin-1-yldiazenyl)benzoate (1013657-95-8) → (E)-N4-(2-(diethylamino)ethyl)-N1-(1-(1-(1-(methoxy(methyl)amino)-4-methyl-1-oxopentan-2-ylamino)-4-methyl-1-oxopentan-2-ylamino)-4-methyl-1-oxopentan-2-yl)-2-(pyrrolidin-1-yldiazenyl)terephthalamide (1013658-00-8)

Guidance literature:

lithium (E)-4-(((2-diethylamino)ethyl)carbamoyl)-2-(pyrrolidin-1-yldiazenyl)benzoate; With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 1h;

(S)-2-Amino-4-methyl-pentanoic acid {(S)-1-[(S)-1-(methoxy-methyl-carbamoyl)-3-methyl-butylcarbamoyl]-3-methyl-butyl}-amide; compound with trifluoro-acetic acid; In dichloromethane; at 20 ℃; Further stages.;

DOI:10.1021/jm701419g

Reference yield: 77.0%

(E)-N4-(2-(diethylamino)ethyl)-N1-(1-(1-(1-(methoxy(methyl)amino)-4-methyl-1-oxopentan-2-ylamino)-4-methyl-1-oxopentan-2-ylamino)-4-methyl-1-oxopentan-2-yl)-2-(pyrrolidin-1-yldiazenyl)terephthalamide (1013658-00-8) → N4-(2-(diethylamino)ethyl)-2-iodo-N1-(1-(1-(1-(methoxy(methyl)amino)-4-methyl-1-oxopentan-2-ylamino)-4-methyl-1-oxopentan-2-ylamino)-4-methyl-1-oxopentan-2-yl)terephthalamide (1013657-98-1)

Guidance literature:

With trifluoroacetic acid; sodium iodide; In acetonitrile; at 20 ℃;

DOI:10.1021/jm701419g

Reference yield: 72.0%

(E)-N4-(2-(diethylamino)ethyl)-N1-(1-(1-(1-(methoxy(methyl)amino)-4-methyl-1-oxopentan-2-ylamino)-4-methyl-1-oxopentan-2-ylamino)-4-methyl-1-oxopentan-2-yl)-2-(pyrrolidin-1-yldiazenyl)terephthalamide (1013658-00-8) → N4-(2-(diethylamino)ethyl)-2-iodo-N1-(4-methyl-1-(4-methyl-1-(4-methyl-1-oxopentan-2-ylamino)-1-oxopentan-2-ylamino)-1-oxopentan-2-yl)terephthalamide (1013658-07-5)

Guidance literature:

With sodium (12?I)iodide; trifluoroacetic acid; sodium iodide; In acetonitrile; at 20 ℃;

DOI:10.1021/jm701419g

upstream raw materials:

lithium (E)-4-(((2-diethylamino)ethyl)carbamoyl)-2-(pyrrolidin-1-yldiazenyl)benzoate

Downstream raw materials:

N⁴-(2-(diethylamino)ethyl)-2-iodo-N¹-(1-(1-(1-(methoxy(methyl)amino)-4-methyl-1-oxopentan-2-ylamino)-4-methyl-1-oxopentan-2-ylamino)-4-methyl-1-oxopentan-2-yl)terephthalamide

C₃₆H₆₀N₈O₅

N⁴-(2-(diethylamino)ethyl)-2-iodo-N¹-(4-methyl-1-(4-methyl-1-(4-methyl-1-oxopentan-2-ylamino)-1-oxopentan-2-ylamino)-1-oxopentan-2-yl)terephthalamide

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