dimethyl 2-phenyl-cyclohexane-1,4-dicarboxylate

Base Information

Chemical Name:dimethyl 2-phenyl-cyclohexane-1,4-dicarboxylate
CAS No.:1257982-60-7
Molecular Formula:C₁₆H₂₀O₄
Molecular Weight:276.332
Hs Code.:

Synonyms:dimethyl 2-phenyl-cyclohexane-1,4-dicarboxylate

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Chemical Property of dimethyl 2-phenyl-cyclohexane-1,4-dicarboxylate

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Technology Process of dimethyl 2-phenyl-cyclohexane-1,4-dicarboxylate

There total 6 articles about dimethyl 2-phenyl-cyclohexane-1,4-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 1119-43-3
(E,E)-hexa-2,4-dienedioic acid dimethyl ester

: 1257982-60-7
dimethyl 2-phenyl-cyclohexane-1,4-dicarboxylate

: 84269-70-5
biphenyl-2,5-dicarboxylic acid dimethyl ester

Guidance literature:: styrene; (E,E)-hexa-2,4-dienedioic acid dimethyl ester; With aluminum oxide; In diethylene glycol dimethyl ether; at 150 ℃; for 24h; Sealed tube;

5% palladium on Al₂O₃; In Triethylene glycol dimethyl ether; for 63h; Inert atmosphere; Reflux;

Reference yield:

: 1257982-61-8
dimethyl 2-phenylcyclohex-5-ene-1,4-dicarboxylate

: 1257982-60-7
dimethyl 2-phenyl-cyclohexane-1,4-dicarboxylate

: 84269-70-5
biphenyl-2,5-dicarboxylic acid dimethyl ester

Guidance literature:: 5 % alumina-supported palladium; In diethylene glycol dimethyl ether; for 63h; Reflux; Inert atmosphere;

Reference yield:

: 1119-72-8
cis,cis-Muconic acid

: 1257982-60-7
dimethyl 2-phenyl-cyclohexane-1,4-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: iodine / acetonitrile / 36 h / Reflux; Ambient light

2.1: sulfuric acid / 16 h / Reflux

3.1: aluminum oxide / diethylene glycol dimethyl ether / 24 h / 150 °C / Sealed tube

3.2: 63 h / Inert atmosphere; Reflux

With aluminum oxide; sulfuric acid; iodine; In diethylene glycol dimethyl ether; acetonitrile;