N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-isopropylhydrazine

Base Information

Chemical Name:N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-isopropylhydrazine
CAS No.:886055-97-6
Molecular Formula:C₂₂H₃₃FN₂O₄
Molecular Weight:408.513
Hs Code.:

Synonyms:N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-isopropylhydrazine

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Chemical Property of N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-isopropylhydrazine

Chemical Property:

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Technology Process of N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-isopropylhydrazine

There total 3 articles about N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-isopropylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 843651-78-5
N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]hydrazine

: 886055-97-6
N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-isopropylhydrazine

Guidance literature:: N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]hydrazine; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.333333h;

isopropyl halide; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/jm050538l

Reference yield:

: 350-40-3
2-(4-fluorophenyl)-1-propene

: 886055-97-6
N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-isopropylhydrazine

Guidance literature:: Multi-step reaction with 3 steps

1.1: NBS / CCl₄ / Heating

2.1: NaH / dimethylformamide / 0.33 h / 20 °C

2.2: 89 percent / dimethylformamide / 7 h / 20 °C

3.1: NaH / dimethylformamide / 0.33 h / 20 °C

3.2: 90 percent / dimethylformamide / 20 °C

With N-Bromosuccinimide; sodium hydride; In tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm050538l

Reference yield:

: 132927-05-0
1-(3-bromoprop-1-en-2-yl)-4-fluorobenzene

: 886055-97-6
N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-isopropylhydrazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / dimethylformamide / 0.33 h / 20 °C

1.2: 89 percent / dimethylformamide / 7 h / 20 °C

2.1: NaH / dimethylformamide / 0.33 h / 20 °C

2.2: 90 percent / dimethylformamide / 20 °C

With sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1021/jm050538l