methyl 12-amino-3-phenyl-4,8-diazadodecanoate

Base Information

Chemical Name:methyl 12-amino-3-phenyl-4,8-diazadodecanoate
CAS No.:209183-01-7
Molecular Formula:C₁₇H₂₉N₃O₂
Molecular Weight:307.436
Hs Code.:

Synonyms:methyl 12-amino-3-phenyl-4,8-diazadodecanoate

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Chemical Property of methyl 12-amino-3-phenyl-4,8-diazadodecanoate

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Technology Process of methyl 12-amino-3-phenyl-4,8-diazadodecanoate

There total 8 articles about methyl 12-amino-3-phenyl-4,8-diazadodecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 163083-85-0
(S)-3-[3-(3-Cyano-propylamino)-propylamino]-3-phenyl-propionic acid methyl ester

: 209183-01-7
methyl 12-amino-3-phenyl-4,8-diazadodecanoate

Guidance literature:: With hydrogenchloride; hydrogen; platinum(IV) oxide; In methanol; at 25 ℃; for 4h; under 760 Torr;
DOI:10.1246/bcsj.71.1221

Reference yield:

: 163083-81-6
methyl (S)-3-(benzhydrylamino)-3-phenylpropionate

: 209183-01-7
methyl 12-amino-3-phenyl-4,8-diazadodecanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / H₂ / Pd/C / methanol / 2.5 h / 25 °C / 760 Torr

2: 92 percent / N,N-diisopropylethylamine / CH₂Cl₂ / 16 h / -78 - 25 °C

3: hydrogen / Pd/C / methanol / 0.5 h / 25 °C / 760 Torr

4: 79 mg / conc. HCl; hydrogen / PtO₂ / methanol / 4 h / 25 °C / 760 Torr

With hydrogenchloride; hydrogen; N-ethyl-N,N-diisopropylamine; platinum(IV) oxide; palladium on activated charcoal; In methanol; dichloromethane; 1: Catalytic hydrogenation / 2: Alkylation / 3: Hydrogenolysis / 4: Catalytic hydrogenation;
DOI:10.1246/bcsj.71.1221

Reference yield:

: 37088-66-7
(3S)-methyl 3-amino-3-phenylpropanoate

: 209183-01-7
methyl 12-amino-3-phenyl-4,8-diazadodecanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / N,N-diisopropylethylamine / CH₂Cl₂ / 16 h / -78 - 25 °C

2: hydrogen / Pd/C / methanol / 0.5 h / 25 °C / 760 Torr

3: 79 mg / conc. HCl; hydrogen / PtO₂ / methanol / 4 h / 25 °C / 760 Torr

With hydrogenchloride; hydrogen; N-ethyl-N,N-diisopropylamine; platinum(IV) oxide; palladium on activated charcoal; In methanol; dichloromethane; 1: Alkylation / 2: Hydrogenolysis / 3: Catalytic hydrogenation;
DOI:10.1246/bcsj.71.1221