(3S)-Bis<4-(tert-butyldiphenylsilyloxy)-3-<(4-methylphenyl)sulfonylamino>butyl>amin

Base Information

Chemical Name:(3S)-Bis<4-(tert-butyldiphenylsilyloxy)-3-<(4-methylphenyl)sulfonylamino>butyl>amin
CAS No.:124921-86-4
Molecular Formula:C₅₄H₆₉N₃O₆S₂Si₂
Molecular Weight:976.461
Hs Code.:

Synonyms:(3S)-Bis<4-(tert-butyldiphenylsilyloxy)-3-<(4-methylphenyl)sulfonylamino>butyl>amin

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Chemical Property of (3S)-Bis<4-(tert-butyldiphenylsilyloxy)-3-<(4-methylphenyl)sulfonylamino>butyl>amin

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Technology Process of (3S)-Bis<4-(tert-butyldiphenylsilyloxy)-3-<(4-methylphenyl)sulfonylamino>butyl>amin

There total 13 articles about (3S)-Bis<4-(tert-butyldiphenylsilyloxy)-3-<(4-methylphenyl)sulfonylamino>butyl>amin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 36212-66-5
N²-(toluene-4-sulfonyl)-L-asparagine

: 124921-86-4
(3S)-Bis<4-(tert-butyldiphenylsilyloxy)-3-<(4-methylphenyl)sulfonylamino>butyl>amin

Guidance literature:: Multi-step reaction with 5 steps

1: 85 percent / Sulfurylchlorid / 72 h / Ambient temperature

2: 1) NOHSO₄, 2) Harnstoff / 1) glacial acetic acid, 30 min, room temperature, 2) 1 h

3: 1) Carbonyldiimidazol / 1) CH₂Cl₂, ca. 45 min, room temperature, 2) 90 min

4: 33 percent / BH₃ / tetrahydrofuran / 1.33 h / Heating

With sulfuryl dichloride; Carbonyldiimidazole; nitrosylsulfuric acid; borane; urea; In tetrahydrofuran;

Reference yield:

: 59642-37-4
N-(p-toluenesulfonyl)L-asparagine methyl ester

: 124921-86-4
(3S)-Bis<4-(tert-butyldiphenylsilyloxy)-3-<(4-methylphenyl)sulfonylamino>butyl>amin

Guidance literature:: Multi-step reaction with 4 steps

1: 1) NOHSO₄, 2) Harnstoff / 1) glacial acetic acid, 30 min, room temperature, 2) 1 h

2: 1) Carbonyldiimidazol / 1) CH₂Cl₂, ca. 45 min, room temperature, 2) 90 min

3: 33 percent / BH₃ / tetrahydrofuran / 1.33 h / Heating

With Carbonyldiimidazole; nitrosylsulfuric acid; borane; urea; In tetrahydrofuran;

Reference yield:

: 124921-80-8
(S)-N-<(4-Methylphenyl)sulfonyl>asparaginsaeure-1-methylester

: 124921-86-4
(3S)-Bis<4-(tert-butyldiphenylsilyloxy)-3-<(4-methylphenyl)sulfonylamino>butyl>amin

Guidance literature:: Multi-step reaction with 3 steps

1: 1) Carbonyldiimidazol / 1) CH₂Cl₂, ca. 45 min, room temperature, 2) 90 min

2: 33 percent / BH₃ / tetrahydrofuran / 1.33 h / Heating

With Carbonyldiimidazole; borane; In tetrahydrofuran;