(2E,2'E)-1,1'-(5,5'-(piperazine-1,4-diylbis(methylene))bis(4-hydroxy-3-methoxy-5,1-phenylene))bis(3-(2-chlorophenyl)prop-2-en-1-one)

Base Information

Chemical Name:(2E,2'E)-1,1'-(5,5'-(piperazine-1,4-diylbis(methylene))bis(4-hydroxy-3-methoxy-5,1-phenylene))bis(3-(2-chlorophenyl)prop-2-en-1-one)
CAS No.:1369787-22-3
Molecular Formula:C₃₈H₃₆Cl₂N₂O₆
Molecular Weight:687.62
Hs Code.:

Synonyms:(2E,2'E)-1,1'-(5,5'-(piperazine-1,4-diylbis(methylene))bis(4-hydroxy-3-methoxy-5,1-phenylene))bis(3-(2-chlorophenyl)prop-2-en-1-one)

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Chemical Property of (2E,2'E)-1,1'-(5,5'-(piperazine-1,4-diylbis(methylene))bis(4-hydroxy-3-methoxy-5,1-phenylene))bis(3-(2-chlorophenyl)prop-2-en-1-one)

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Technology Process of (2E,2'E)-1,1'-(5,5'-(piperazine-1,4-diylbis(methylene))bis(4-hydroxy-3-methoxy-5,1-phenylene))bis(3-(2-chlorophenyl)prop-2-en-1-one)

There total 2 articles about (2E,2'E)-1,1'-(5,5'-(piperazine-1,4-diylbis(methylene))bis(4-hydroxy-3-methoxy-5,1-phenylene))bis(3-(2-chlorophenyl)prop-2-en-1-one) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1369787-34-7
C₂₄H₃₀N₂O₆

: 89-98-5
2-chloro-benzaldehyde

: 1369787-22-3
(2E,2'E)-1,1'-(5,5'-(piperazine-1,4-diylbis(methylene))bis(4-hydroxy-3-methoxy-5,1-phenylene))bis(3-(2-chlorophenyl)prop-2-en-1-one)

Guidance literature:: With potassium hydroxide; In methanol; at 0 - 20 ℃;
DOI:10.1248/cpb.59.1549

Reference yield:

: 498-02-2
1-(3-methoxy-4-hydroxyphenyl)ethanone

: 1369787-22-3
(2E,2'E)-1,1'-(5,5'-(piperazine-1,4-diylbis(methylene))bis(4-hydroxy-3-methoxy-5,1-phenylene))bis(3-(2-chlorophenyl)prop-2-en-1-one)

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 20 h / 120 °C

2: potassium hydroxide / methanol / 0 - 20 °C

With potassium hydroxide; In methanol; ethanol; 1: Mannich reaction / 2: Claisen Schmidt condensation;
DOI:10.1248/cpb.59.1549