(+/-)9-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>guanine

Base Information

Chemical Name:(+/-)9-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>guanine
CAS No.:136083-17-5
Molecular Formula:C₂₆H₃₁N₅O₃Si
Molecular Weight:489.649
Hs Code.:

Synonyms:(+/-)9-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>guanine

Suppliers and Price of (+/-)9-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>guanine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)9-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>guanine

Chemical Property:

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Technology Process of (+/-)9-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>guanine

There total 5 articles about (+/-)9-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>guanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 130372-35-9
2-Amino-9-trimethylsilanyl-1,9-dihydro-purin-6-one

: 136083-14-2
(+/-)-1-tert-Butyldiphenylsilyloxy-2-acetoxymethylenoxybut-3-ene

: 136083-17-5
(+/-)9-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>guanine

Guidance literature:: With dibenzo-18-crown-6; potassium iodide; In toluene; acetonitrile; at 80 ℃; for 4h; solid-liquid phase transfer catalysis;

Reference yield:

: 73-40-5
2-amino-1,9-dihydro-6H-purin-6-one

: 136083-17-5
(+/-)9-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>guanine

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium sulfate / 48 h / Heating

2: 98 percent / dibenzo-18-crown-6 ether, KI / acetonitrile; toluene / 4 h / 80 °C / solid-liquid phase transfer catalysis

With ammonium sulfate; dibenzo-18-crown-6; potassium iodide; In toluene; acetonitrile;

Reference yield:

: 177032-63-2
(+/-)-1-(tert-butyldiphenylsilyloxy)-2-hydroxy-3-butene

: 136083-17-5
(+/-)9-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>guanine

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / P₂O₅ / CHCl₃ / 24 h / Ambient temperature

2: 95 percent / BF₃*Et₂O / diethyl ether / 48 h / 4 °C

3: 98 percent / dibenzo-18-crown-6 ether, KI / acetonitrile; toluene / 4 h / 80 °C / solid-liquid phase transfer catalysis

With dibenzo-18-crown-6; boron trifluoride diethyl etherate; phosphorus pentoxide; potassium iodide; In diethyl ether; chloroform; toluene; acetonitrile;