2-(benzyloxycarbonyl)aminoethyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-α-D-mannopyranoside

Base Information

Chemical Name:2-(benzyloxycarbonyl)aminoethyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-α-D-mannopyranoside
CAS No.:497096-20-5
Molecular Formula:C₃₂H₃₈N₂O₈
Molecular Weight:578.662
Hs Code.:

Synonyms:2-(benzyloxycarbonyl)aminoethyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-α-D-mannopyranoside

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Chemical Property of 2-(benzyloxycarbonyl)aminoethyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-α-D-mannopyranoside

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Technology Process of 2-(benzyloxycarbonyl)aminoethyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-α-D-mannopyranoside

There total 8 articles about 2-(benzyloxycarbonyl)aminoethyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1160939-17-2
C₃₈H₅₂N₂O₈Si

: 497096-20-5
2-(benzyloxycarbonyl)aminoethyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-α-D-mannopyranoside

Guidance literature:: With tetrabutyl ammonium fluoride;

Reference yield: 93.0%

: 497096-19-2
2-(benzyloxycarbonyl)aminoethyl 2-acetamido-6-O-acetyl-3,4-di-O-benzyl-2-deoxy-α-D-mannopyranoside

: 497096-20-5
2-(benzyloxycarbonyl)aminoethyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-α-D-mannopyranoside

Guidance literature:: With sodium methylate; In methanol; at 23 ℃; for 0.5h;
DOI:10.1002/1521-3765(20021004)8:19<4424::AID-CHEM4424>3.0.CO;2-1

Reference yield:

: 77987-49-6
benzyl 2-hydroxyethylcarbamate

: 497096-20-5
2-(benzyloxycarbonyl)aminoethyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 54 percent / TMSOTf / CH₂Cl₂ / 0.5 h / 0 °C

2: NaBH₄; NiCl₂*6H₂O / methanol / 1 h / 0 - 10 °C

3: 8.15 g / methanol / 0.5 h / 5 °C

4: 93 percent / NaOMe / methanol / 0.5 h / 23 °C

With sodium tetrahydroborate; trimethylsilyl trifluoromethanesulfonate; sodium methylate; nickel dichloride; In methanol; dichloromethane;
DOI:10.1002/1521-3765(20021004)8:19<4424::AID-CHEM4424>3.0.CO;2-1