i-butyl 4-(biphenyl-4-yl)-2,7,7-trimethyl-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate

Base Information

Chemical Name:i-butyl 4-(biphenyl-4-yl)-2,7,7-trimethyl-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate
CAS No.:1408382-23-9
Molecular Formula:C₂₉H₃₃NO₃
Molecular Weight:443.586
Hs Code.:

Synonyms:i-butyl 4-(biphenyl-4-yl)-2,7,7-trimethyl-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate

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Chemical Property of i-butyl 4-(biphenyl-4-yl)-2,7,7-trimethyl-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate

Chemical Property:

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Technology Process of i-butyl 4-(biphenyl-4-yl)-2,7,7-trimethyl-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate

There total 5 articles about i-butyl 4-(biphenyl-4-yl)-2,7,7-trimethyl-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 78-77-3
Isobutyl bromide

: 1394961-64-8,1394961-65-9,1408382-80-8
4-([1,1’-biphenyl]-4-yl)-2,7,7-trimethyl-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylic acid

: 1408382-23-9
i-butyl 4-(biphenyl-4-yl)-2,7,7-trimethyl-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.ejmech.2015.03.027

Reference yield:

: 7779-75-1
isobutyl acetoacetate

: 126-81-8
dimedone

: 3218-36-8
4-Phenylbenzaldehyde

: 1408382-23-9
i-butyl 4-(biphenyl-4-yl)-2,7,7-trimethyl-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate

Guidance literature:: With ammonium acetate; iodine; In ethanol; at 20 ℃;
DOI:10.1021/jm301144g

Reference yield:

: 1099644-42-4,1169983-42-9,1394961-38-6
ethyl 2,7,7-trimethyl-5-oxo-4-(4-phenylphenyl)-1,4,5,6,7,8-hexahydro-3-quinolinecarboxylate

: 1408382-23-9
i-butyl 4-(biphenyl-4-yl)-2,7,7-trimethyl-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: boron trichloride / dichloromethane / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 20 °C

With boron trichloride; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2015.03.027