Technology Process of 12-acetoxy-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone
There total 6 articles about 12-acetoxy-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid;
In
ethanol; benzene;
for 8h;
Inert atmosphere;
Reflux;
DOI:10.1016/j.tet.2012.10.071
- Guidance literature:
-
Multi-step reaction with 2 steps
1: chromium(VI) oxide; tert.-butylhydroperoxide / dichloromethane; pyridine / 25 h / 20 °C
2: toluene-4-sulfonic acid / benzene; ethanol / 8 h / Inert atmosphere; Reflux
With
chromium(VI) oxide; tert.-butylhydroperoxide; toluene-4-sulfonic acid;
In
pyridine; ethanol; dichloromethane; benzene;
DOI:10.1016/j.tet.2012.10.071
- Guidance literature:
-
Multi-step reaction with 5 steps
1: acetic acid / 2.5 h / 130 °C / Inert atmosphere
2: aluminum (III) chloride / carbon disulfide / 5 h / Inert atmosphere; Reflux
3: 3-chloro-benzenecarboperoxoic acid; toluene-4-sulfonic acid / dichloromethane / 48 h / 20 °C
4: chromium(VI) oxide; tert.-butylhydroperoxide / dichloromethane; pyridine / 25 h / 20 °C
5: toluene-4-sulfonic acid / benzene; ethanol / 8 h / Inert atmosphere; Reflux
With
chromium(VI) oxide; tert.-butylhydroperoxide; aluminum (III) chloride; toluene-4-sulfonic acid; acetic acid; 3-chloro-benzenecarboperoxoic acid;
In
pyridine; carbon disulfide; ethanol; dichloromethane; benzene;
DOI:10.1016/j.tet.2012.10.071
