12-acetoxy-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone

Base Information

Chemical Name:12-acetoxy-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone
CAS No.:1415684-67-1
Molecular Formula:C₃₇H₃₇Cl₄N₃O₆S
Molecular Weight:793.595
Hs Code.:

Synonyms:12-acetoxy-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone

Suppliers and Price of 12-acetoxy-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 12-acetoxy-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 12-acetoxy-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone

There total 6 articles about 12-acetoxy-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1415684-63-7
12-acetoxy-7-oxo-N,N-(tetrachlorophthaloyl)dehydroabietylamine

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 1415684-67-1
12-acetoxy-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone

Guidance literature:: With toluene-4-sulfonic acid; In ethanol; benzene; for 8h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2012.10.071

Reference yield:

: 1415684-59-1
(4R)-12-acetoxy-N,N-(tetrachlorophthaloyl)dehydroabietylamine

: 1415684-67-1
12-acetoxy-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: chromium(VI) oxide; tert.-butylhydroperoxide / dichloromethane; pyridine / 25 h / 20 °C

2: toluene-4-sulfonic acid / benzene; ethanol / 8 h / Inert atmosphere; Reflux

With chromium(VI) oxide; tert.-butylhydroperoxide; toluene-4-sulfonic acid; In pyridine; ethanol; dichloromethane; benzene;
DOI:10.1016/j.tet.2012.10.071

Reference yield:

: 117-08-8
tetrachlorophthalic anhydride

: 1415684-67-1
12-acetoxy-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid / 2.5 h / 130 °C / Inert atmosphere

2: aluminum (III) chloride / carbon disulfide / 5 h / Inert atmosphere; Reflux

3: 3-chloro-benzenecarboperoxoic acid; toluene-4-sulfonic acid / dichloromethane / 48 h / 20 °C

4: chromium(VI) oxide; tert.-butylhydroperoxide / dichloromethane; pyridine / 25 h / 20 °C

5: toluene-4-sulfonic acid / benzene; ethanol / 8 h / Inert atmosphere; Reflux

With chromium(VI) oxide; tert.-butylhydroperoxide; aluminum (III) chloride; toluene-4-sulfonic acid; acetic acid; 3-chloro-benzenecarboperoxoic acid; In pyridine; carbon disulfide; ethanol; dichloromethane; benzene;
DOI:10.1016/j.tet.2012.10.071