3-(3-chloropropylbenzyloxycarbonylsulfonamide)-2-methoxy-1-octadecylcarbamoyloxypropane

Base Information

Chemical Name:3-(3-chloropropylbenzyloxycarbonylsulfonamide)-2-methoxy-1-octadecylcarbamoyloxypropane
CAS No.:140685-51-4
Molecular Formula:C₃₄H₅₉ClN₂O₇S
Molecular Weight:675.371
Hs Code.:

Synonyms:3-(3-chloropropylbenzyloxycarbonylsulfonamide)-2-methoxy-1-octadecylcarbamoyloxypropane

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Chemical Property of 3-(3-chloropropylbenzyloxycarbonylsulfonamide)-2-methoxy-1-octadecylcarbamoyloxypropane

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Technology Process of 3-(3-chloropropylbenzyloxycarbonylsulfonamide)-2-methoxy-1-octadecylcarbamoyloxypropane

There total 2 articles about 3-(3-chloropropylbenzyloxycarbonylsulfonamide)-2-methoxy-1-octadecylcarbamoyloxypropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 80350-03-4
3-(N-octadecylcarbamoyloxy)-2-methoxy-1-propanol

: 140685-47-8
N-benzyloxycarbonyl-3-chloropropanesulfonamide

: 140685-51-4
3-(3-chloropropylbenzyloxycarbonylsulfonamide)-2-methoxy-1-octadecylcarbamoyloxypropane

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; Ambient temperature;
DOI:10.1248/cpb.40.75

Reference yield:

: 621-84-1
O-benzyl carbamate

: 140685-51-4
3-(3-chloropropylbenzyloxycarbonylsulfonamide)-2-methoxy-1-octadecylcarbamoyloxypropane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) lithium hexamethyldisilazide / 1.) THF, -70 deg C, 1 h, 2.) THF, from -70 deg C to RT

2: 89 percent / PPh₃, diethyl azodicarboxylate (DEAD) / tetrahydrofuran / Ambient temperature

With triphenylphosphine; lithium hexamethyldisilazane; diethylazodicarboxylate; In tetrahydrofuran;
DOI:10.1248/cpb.40.75

Reference yield:

: 140685-51-4
3-(3-chloropropylbenzyloxycarbonylsulfonamide)-2-methoxy-1-octadecylcarbamoyloxypropane

: C₃₂H₅₈N₂O₆SSe

Guidance literature:: Multi-step reaction with 3 steps

1: NH₂NH₂

2: 1.) NaBH₄, 2.) AcOH / 1.) EtOH, 2.) EtOH, THF, RT, 1.5 h

3: H₂O₂, pyridine / CH₂Cl₂; methanol / 5 h / Ambient temperature

With pyridine; sodium tetrahydroborate; dihydrogen peroxide; acetic acid; hydrazine; In methanol; dichloromethane;
DOI:10.1248/cpb.40.75