methyl N-<2-(N-Z)aminoethyl>-N-glycinate

Base Information

Chemical Name:methyl N-<2-(N-Z)aminoethyl>-N-glycinate
CAS No.:221554-78-5
Molecular Formula:C₁₇H₂₂N₂O₆
Molecular Weight:350.371
Hs Code.:

methyl N-<2-(N-Z)aminoethyl>-N-<Alloc>glycinate

Synonyms:methyl N-<2-(N-Z)aminoethyl>-N-glycinate

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Chemical Property of methyl N-<2-(N-Z)aminoethyl>-N-glycinate

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Technology Process of methyl N-<2-(N-Z)aminoethyl>-N-glycinate

There total 1 articles about methyl N-<2-(N-Z)aminoethyl>-N-glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 128421-96-5
methyl N-<2-(N-benzyloxycarbonyl)aminoethyl>glycinate

: 2937-50-0
Allyl chloroformate

: 221554-78-5
methyl N-<2-(N-Z)aminoethyl>-N-glycinate

Guidance literature:: With triethylamine; In dichloromethane; for 1h; Ambient temperature;
DOI:10.1016/S0040-4020(98)01211-3

Reference yield: 93.0%

: 221554-78-5
methyl N-<2-(N-Z)aminoethyl>-N-glycinate

: 221554-80-9
N-<2-(N-Z)aminoethyl>-N-glycine

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1016/S0040-4020(98)01211-3

Reference yield:

: 221554-78-5
methyl N-<2-(N-Z)aminoethyl>-N-glycinate

: 221554-87-6
[allyloxycarbonyl-(2-{2-[(2-{2-[allyloxycarbonyl-(2-benzyloxycarbonylamino-ethyl)-amino]-acetylamino}-ethyl)-(2,2,2-trichloro-ethoxycarbonyl)-amino]-acetylamino}-ethyl)-amino]-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / aq. LiOH / tetrahydrofuran / 1 h / 0 °C

2: 1.) isobutyl chloroformate, 2.) Et₃N / 1.) CH₂Cl₂, -15 deg C, 15 min, 2.) CH₂Cl₂, -15 deg C (3 h), -> room temperature (1 h)

3: 90 percent / aq. LiOH / methanol / 2 h / 0 °C

4: 1.) isobutyl chloroformate, 2.) Et₃N / 1.) CH₂Cl₂, -15 deg C, 15 min, 2.) CH₂Cl₂, -15 deg C (3 h) -> room temperature (1 h)

With lithium hydroxide; triethylamine; isobutyl chloroformate; In tetrahydrofuran; methanol;
DOI:10.1016/S0040-4020(98)01211-3