N-[8-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yloxy)-6-dodecyloxy-2-styryl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

Base Information

• Chemical Name: N-[8-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yloxy)-6-dodecyloxy-2-styryl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide
• CAS No.: 824396-58-9
• Molecular Formula: C₄₄H₅₇NO₆
• Molecular Weight: 695.94

Synonyms:N-[8-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yloxy)-6-dodecyloxy-2-styryl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

Chemical Property of N-[8-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yloxy)-6-dodecyloxy-2-styryl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

Chemical Property:

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Technology Process of N-[8-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yloxy)-6-dodecyloxy-2-styryl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

There total 3 articles about N-[8-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yloxy)-6-dodecyloxy-2-styryl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

5-chlorodibenzosuberane (1210-33-9) + 1-dodecyl 2-acetamido-2-deoxy-(R)-4,6-O-(E-3-phenyl-2-propenylidene)-β-D-glucopyranoside (824396-41-0) → N-[8-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yloxy)-6-dodecyloxy-2-styryl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide (824396-58-9)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 48h;

DOI:10.1016/j.tetasy.2004.09.034

Reference yield:

(E)-cinnamaldehyde dimethylacetal (4364-06-1) → N-[8-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yloxy)-6-dodecyloxy-2-styryl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide (824396-58-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / anhydrous camphorsulfonic acid / acetonitrile / 20 °C

2: 64 percent / triethylamine / CH₂Cl₂ / 48 h / 20 °C

With camphor-10-sulfonic acid; triethylamine; In dichloromethane; acetonitrile;

DOI:10.1016/j.tetasy.2004.09.034

Reference yield:

dodecyl 2-(acetylamino)-2-deoxy-β-D-glucopyranoside (147025-06-7) → N-[8-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yloxy)-6-dodecyloxy-2-styryl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide (824396-58-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / anhydrous camphorsulfonic acid / acetonitrile / 20 °C

2: 64 percent / triethylamine / CH₂Cl₂ / 48 h / 20 °C

With camphor-10-sulfonic acid; triethylamine; In dichloromethane; acetonitrile;

DOI:10.1016/j.tetasy.2004.09.034

upstream raw materials:

5-chlorodibenzosuberane

1-dodecyl 2-acetamido-2-deoxy-(R)-4,6-O-(E-3-phenyl-2-propenylidene)-β-D-glucopyranoside

(E)-cinnamaldehyde dimethylacetal

dodecyl 2-(acetylamino)-2-deoxy-β-D-glucopyranoside

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