[(S)-6-(2-Bromo-3-dimethoxymethyl-6-methoxy-phenoxy)-cyclohex-1-enyl]-acetonitrile

Base Information

Chemical Name:[(S)-6-(2-Bromo-3-dimethoxymethyl-6-methoxy-phenoxy)-cyclohex-1-enyl]-acetonitrile
CAS No.:869369-38-0
Molecular Formula:C₁₈H₂₂BrNO₄
Molecular Weight:396.281
Hs Code.:

Synonyms:[(S)-6-(2-Bromo-3-dimethoxymethyl-6-methoxy-phenoxy)-cyclohex-1-enyl]-acetonitrile

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Chemical Property of [(S)-6-(2-Bromo-3-dimethoxymethyl-6-methoxy-phenoxy)-cyclohex-1-enyl]-acetonitrile

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Technology Process of [(S)-6-(2-Bromo-3-dimethoxymethyl-6-methoxy-phenoxy)-cyclohex-1-enyl]-acetonitrile

There total 1 articles about [(S)-6-(2-Bromo-3-dimethoxymethyl-6-methoxy-phenoxy)-cyclohex-1-enyl]-acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-86-5
2-hydroxy-2-methylpropanenitrile

: 482374-40-3
[6-(2-bromo-3-dimethoxymethyl-6-methoxyphenoxy)cyclohex-1-enyl]methanol

: 869369-38-0
[(S)-6-(2-Bromo-3-dimethoxymethyl-6-methoxy-phenoxy)-cyclohex-1-enyl]-acetonitrile

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In diethyl ether;
DOI:10.1002/1521-3773(20020802)41:15<2795::AID-ANIE2795>3.0.CO;2-2

Reference yield:

: 869369-38-0
[(S)-6-(2-Bromo-3-dimethoxymethyl-6-methoxy-phenoxy)-cyclohex-1-enyl]-acetonitrile

: 357-70-0
Galantamine

Guidance literature:: Multi-step reaction with 6 steps

1: p-toluenesolfonic acid; water / tetrahydrofuran

2: 91 percent / Pd(OAc)2; bis(diphenylphosphanyl)propane; Ag₂CO₃ / toluene / 24 h / 107 °C

3: 57 percent / SeO₂; NaH₂PO₄ / dioxane / 3 h / 150 °C

4: methanol

5: diisobutylaluminum hydride

6: sodium cyanoborohydride / H₂O

With palladium diacetate; sodium dihydrogenphosphate; selenium(IV) oxide; 1,3-bis-(diphenylphosphino)propane; water; diisobutylaluminium hydride; sodium cyanoborohydride; toluene-4-sulfonic acid; silver carbonate; In tetrahydrofuran; 1,4-dioxane; methanol; water; toluene; 2: intramolecular Heck reaction;
DOI:10.1002/1521-3773(20020802)41:15<2795::AID-ANIE2795>3.0.CO;2-2