9-{2'-O-[(4'',4'''-dimethoxytriphenyl)methyl]-α-L-arabinopyranosyl}-N²-(phenoxyacetyl)adenine

Base Information

• Chemical Name: 9-{2'-O-[(4'',4'''-dimethoxytriphenyl)methyl]-α-L-arabinopyranosyl}-N²-(phenoxyacetyl)adenine
• CAS No.: 619276-83-4
• Molecular Formula: C₃₉H₃₇N₅O₈
• Molecular Weight: 703.751

Synonyms:9-{2'-O-[(4'',4'''-dimethoxytriphenyl)methyl]-α-L-arabinopyranosyl}-N²-(phenoxyacetyl)adenine

Chemical Property of 9-{2'-O-[(4'',4'''-dimethoxytriphenyl)methyl]-α-L-arabinopyranosyl}-N²-(phenoxyacetyl)adenine

Chemical Property:

Purity/Quality:

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Technology Process of 9-{2'-O-[(4'',4'''-dimethoxytriphenyl)methyl]-α-L-arabinopyranosyl}-N²-(phenoxyacetyl)adenine

There total 10 articles about 9-{2'-O-[(4'',4'''-dimethoxytriphenyl)methyl]-α-L-arabinopyranosyl}-N²-(phenoxyacetyl)adenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(9-{7-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-2-dimethylamino-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-yl}-9H-purin-6-yl)-2-phenoxy-acetamide → 9-{2'-O-[(4'',4'''-dimethoxytriphenyl)methyl]-α-L-arabinopyranosyl}-N2-(phenoxyacetyl)adenine (619276-83-4)

Guidance literature:

With sodium hydrogencarbonate; citric acid; In dichloromethane; water;

DOI:10.1002/hlca.200390118

Reference yield:

9-(α-L-arabinopyranosyl)adenine (17434-53-6) → 9-{2'-O-[(4'',4'''-dimethoxytriphenyl)methyl]-α-L-arabinopyranosyl}-N2-(phenoxyacetyl)adenine (619276-83-4)

Guidance literature:

Multi-step reaction with 6 steps

1: pyridine / 0.5 h / 20 °C

2: 1-HOBT / pyridine; CH₂Cl₂ / 20 °C

3: 5.8 g / H₂O

4: pyridine; dimethylformamide / 1 h / 0 °C

5: collodine / pyridine / 6 h / 20 °C

6: 8.1 g / NaHCO₃; citric acid / H₂O; CH₂Cl₂

With collodine; water; sodium hydrogencarbonate; benzotriazol-1-ol; citric acid; In pyridine; dichloromethane; water; N,N-dimethyl-formamide;

DOI:10.1002/hlca.200390118

Reference yield:

4,4'-dimethoxytrityl chloride (40615-36-9) → 9-{2'-O-[(4'',4'''-dimethoxytriphenyl)methyl]-α-L-arabinopyranosyl}-N2-(phenoxyacetyl)adenine (619276-83-4)

Guidance literature:

Multi-step reaction with 2 steps

1: collodine / pyridine / 6 h / 20 °C

2: 8.1 g / NaHCO₃; citric acid / H₂O; CH₂Cl₂

With collodine; sodium hydrogencarbonate; citric acid; In pyridine; dichloromethane; water;

DOI:10.1002/hlca.200390118

upstream raw materials:

9-(α-L-arabinopyranosyl)adenine

4,4'-dimethoxytrityl chloride

N-benzoyladenine

9-(α-L-arabinopyranosyl)-N²-(phenoxyacetyl)adenine

Downstream raw materials:

9-{4'-O-benzoyl-2'-O-[(4'',4'''-dimethoxytriphenyl)methyl]-α-L-arabinopyranosyl}-N²-(phenoxyacetyl)adenine

9-{3'-O-benzoyl-2'-O-[(4'',4'''-dimethoxytriphenyl)methyl]-α-L-arabinopyranosyl}-N²-(phenoxyacetyl)adenine

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