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Technology Process of methyl O2-benzoyl-O3t-butoxycarbonyl-O4-diphenylphosphoryl-O6-p-toluenesulfonyl-α-Dglucoside

methyl O2-benzoyl-O3t-butoxycarbonyl-O4-diphenylphosphoryl-O6-p-toluenesulfonyl-α-Dglucoside

Base Information
  • Chemical Name:methyl O2-benzoyl-O3t-butoxycarbonyl-O4-diphenylphosphoryl-O6-p-toluenesulfonyl-α-Dglucoside
  • CAS No.:1073186-63-6
  • Molecular Formula:C38H41O14PS
  • Molecular Weight:784.775
  • Hs Code.:
methyl O<sup>2</sup>-benzoyl-O<sup>3</sup>t-butoxycarbonyl-O<sup>4</sup>-diphenylphosphoryl-O<sup>6</sup>-p-toluenesulfonyl-α-Dglucoside

Synonyms:methyl O2-benzoyl-O3t-butoxycarbonyl-O4-diphenylphosphoryl-O6-p-toluenesulfonyl-α-Dglucoside

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Chemical Property of methyl O2-benzoyl-O3t-butoxycarbonyl-O4-diphenylphosphoryl-O6-p-toluenesulfonyl-α-Dglucoside
Chemical Property:
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Technology Process of methyl O2-benzoyl-O3t-butoxycarbonyl-O4-diphenylphosphoryl-O6-p-toluenesulfonyl-α-Dglucoside

There total 1 articles about methyl O2-benzoyl-O3t-butoxycarbonyl-O4-diphenylphosphoryl-O6-p-toluenesulfonyl-α-Dglucoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

methyl O<sup>2</sup>-benzoyl-O<sup>3</sup>-t-butoxycarbonyl-O<sup>6</sup>-p-toluenesulfonyl-α-D-glucoside
1073186-62-5

methyl O2-benzoyl-O3-t-butoxycarbonyl-O6-p-toluenesulfonyl-α-D-glucoside

chlorophosphoric acid diphenyl ester
2524-64-3

chlorophosphoric acid diphenyl ester

methyl O<sup>2</sup>-benzoyl-O<sup>3</sup>t-butoxycarbonyl-O<sup>4</sup>-diphenylphosphoryl-O<sup>6</sup>-p-toluenesulfonyl-α-Dglucoside
1073186-63-6

methyl O2-benzoyl-O3t-butoxycarbonyl-O4-diphenylphosphoryl-O6-p-toluenesulfonyl-α-Dglucoside

Guidance literature:
With pyridine; dmap; In dichloromethane; at 20 ℃; for 22h;
DOI:10.1021/ol802095e

Reference yield: 95.0%

methyl O<sup>2</sup>-benzoyl-O<sup>3</sup>t-butoxycarbonyl-O<sup>4</sup>-diphenylphosphoryl-O<sup>6</sup>-p-toluenesulfonyl-α-Dglucoside
1073186-63-6

methyl O2-benzoyl-O3t-butoxycarbonyl-O4-diphenylphosphoryl-O6-p-toluenesulfonyl-α-Dglucoside

methyl O<sup>2</sup>-benzoyl-O<sup>3</sup>-t-butoxycarbonyl-O<sup>4</sup>-diphenylphosphoryl-6-deoxy-6-azido-α-D-glucoside
1073186-66-9

methyl O2-benzoyl-O3-t-butoxycarbonyl-O4-diphenylphosphoryl-6-deoxy-6-azido-α-D-glucoside

Guidance literature:
With sodium azide; 15-crown-5; In N,N-dimethyl-formamide; at 50 ℃; for 20h;
DOI:10.1021/ol802095e
upstream raw materials:

methyl O2-benzoyl-O3-t-butoxycarbonyl-O6-p-toluenesulfonyl-α-D-glucoside

chlorophosphoric acid diphenyl ester

Downstream raw materials:

methyl O2-benzoyl-O3-t-butoxycarbonyl-O4-diphenylphosphoryl-6-deoxy-6-azido-α-D-glucoside

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