(S)-benzyl (5-amino-5-(5-(naphthalen-2-yl)-1H-imidazol-2-yl)pentyl)carbamate

Base Information

Chemical Name:(S)-benzyl (5-amino-5-(5-(naphthalen-2-yl)-1H-imidazol-2-yl)pentyl)carbamate
CAS No.:936367-36-1
Molecular Formula:C₂₆H₂₈N₄O₂
Molecular Weight:428.534
Hs Code.:

Synonyms:(S)-benzyl (5-amino-5-(5-(naphthalen-2-yl)-1H-imidazol-2-yl)pentyl)carbamate

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Chemical Property of (S)-benzyl (5-amino-5-(5-(naphthalen-2-yl)-1H-imidazol-2-yl)pentyl)carbamate

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Technology Process of (S)-benzyl (5-amino-5-(5-(naphthalen-2-yl)-1H-imidazol-2-yl)pentyl)carbamate

There total 3 articles about (S)-benzyl (5-amino-5-(5-(naphthalen-2-yl)-1H-imidazol-2-yl)pentyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 936367-35-0
(S)-benzyl tert-butyl (1-(5-(naphthalen-2-yl)-1H-imidazol-2-yl)pentane-1,5-diyl)dicarbamate

: 936367-36-1
(S)-benzyl (5-amino-5-(5-(naphthalen-2-yl)-1H-imidazol-2-yl)pentyl)carbamate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 23 ℃; for 2h;
DOI:10.1021/acsmedchemlett.0c00462

Reference yield:

: 2389-45-9
Boc-Lys(Z)-OH

: 936367-36-1
(S)-benzyl (5-amino-5-(5-(naphthalen-2-yl)-1H-imidazol-2-yl)pentyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / N,N-dimethyl-formamide / 1.08 h / 20 °C

2: ammonium acetate / tert-butyl alcohol / 0.75 h / 90 °C / Sealed tube

3: trifluoroacetic acid / dichloromethane / 2 h / 23 °C

With ammonium acetate; caesium carbonate; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: (S)-2-(naphthalen-2-yl)-2-oxoethyl 6-(((benzyloxy)carbonyl)amino)-2-((tert-butoxycarbonyl)amino)hexanoate

: 936367-36-1
(S)-benzyl (5-amino-5-(5-(naphthalen-2-yl)-1H-imidazol-2-yl)pentyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium acetate / tert-butyl alcohol / 0.75 h / 90 °C / Sealed tube

2: trifluoroacetic acid / dichloromethane / 2 h / 23 °C

With ammonium acetate; trifluoroacetic acid; In dichloromethane; tert-butyl alcohol;