2-(6'-azido-2',3',4'-tri-O-benzoyl-6'-deoxy-β-D-glucopyranosyl)-1,4-dimethoxybenzene

Base Information

• Chemical Name: 2-(6'-azido-2',3',4'-tri-O-benzoyl-6'-deoxy-β-D-glucopyranosyl)-1,4-dimethoxybenzene
• CAS No.: 1093850-32-8
• Molecular Formula: C₃₅H₃₁N₃O₉
• Molecular Weight: 637.646

Synonyms:2-(6'-azido-2',3',4'-tri-O-benzoyl-6'-deoxy-β-D-glucopyranosyl)-1,4-dimethoxybenzene

Chemical Property of 2-(6'-azido-2',3',4'-tri-O-benzoyl-6'-deoxy-β-D-glucopyranosyl)-1,4-dimethoxybenzene

Chemical Property:

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Technology Process of 2-(6'-azido-2',3',4'-tri-O-benzoyl-6'-deoxy-β-D-glucopyranosyl)-1,4-dimethoxybenzene

There total 1 articles about 2-(6'-azido-2',3',4'-tri-O-benzoyl-6'-deoxy-β-D-glucopyranosyl)-1,4-dimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C36H34O12S → 2-(6'-azido-2',3',4'-tri-O-benzoyl-6'-deoxy-β-D-glucopyranosyl)-1,4-dimethoxybenzene (1093850-32-8)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; at 90 ℃; for 20h;

DOI:10.1016/j.bmc.2008.09.066

Reference yield: 94.0%

2-(6'-azido-2',3',4'-tri-O-benzoyl-6'-deoxy-β-D-glucopyranosyl)-1,4-dimethoxybenzene (1093850-32-8) + bis(prop-2-ynyl)benzene-1,3-dicarboxylate (92152-09-5) → C84H72N6O22 (1093850-46-4)

Guidance literature:

With copper(II) sulfate; sodium L-ascorbate; In dichloromethane; water; at 20 ℃;

DOI:10.1016/j.bmc.2008.09.066

Reference yield: 47.0%

phthalic anhydride (85-44-9) + 2-(6'-azido-2',3',4'-tri-O-benzoyl-6'-deoxy-β-D-glucopyranosyl)-1,4-dimethoxybenzene (1093850-32-8) → C43H35NO11 (1101835-12-4) + C43H37NO12 (1101835-11-3)

Guidance literature:

With triphenylphosphine; In dichloromethane;

DOI:10.1016/j.bmcl.2008.10.091

Downstream raw materials:

C₈₄H₇₂N₆O₂₂

C₃₅H₃₃NO₉

C₄₃H₃₅NO₁₁

C₄₃H₃₇NO₁₂

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