ethyl 4-iodomethylbenzoate

Base Information

Chemical Name:ethyl 4-iodomethylbenzoate
CAS No.:73373-16-7
Molecular Formula:C₁₀H₁₁IO₂
Molecular Weight:290.101
Hs Code.:

Synonyms:ethyl 4-iodomethylbenzoate

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Chemical Property of ethyl 4-iodomethylbenzoate

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Technology Process of ethyl 4-iodomethylbenzoate

There total 1 articles about ethyl 4-iodomethylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26496-94-6
Ethyl 4-(bromomethyl)benzoate

: 73373-16-7
ethyl 4-iodomethylbenzoate

Guidance literature:: With sodium iodide; In acetone; for 48h; Heating;
DOI:10.1021/ja00522a042

Reference yield:

: 73373-16-7
ethyl 4-iodomethylbenzoate

: 94-08-6
4-methylbenzoic acid ethyl ester

Guidance literature:: With Perbenzoic acid; tri-n-butyl-tin hydride; In benzene; at 90 ℃; for 12h; Mechanism; in the presence of α-iodotoluene (competitor), relative reactivity;
DOI:10.1021/ja00522a042

Reference yield:

: 73373-16-7
ethyl 4-iodomethylbenzoate

: C₁₅H₁₉ClO₅

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: lithium tri-t-butoxyaluminum hydride / tetrahydrofuran / 12 h / 40 °C / Inert atmosphere

With sodium hydride; lithium tri-t-butoxyaluminum hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jacs.1c12404