Technology Process of 2,3-Dibenzofurandiol, 5a,6,7,8,9,9a-hexahydro-, trans- (9CI)
There total 9 articles about 2,3-Dibenzofurandiol, 5a,6,7,8,9,9a-hexahydro-, trans- (9CI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 52 percent / 60percent NaH in mineral oil / 1,2-dimethoxy-ethane / 16 h / Ambient temperature
2: 1.) Hg(ClO4)2*3H2O; 2.) acetic acid / 1.) THF, chloroform, r.t., 15 min; 2.) reflux, 1 h
With
mercury(II) perchlorate; sodium hydride; acetic acid;
In
1,2-dimethoxyethane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 38 percent / 60percent NaH in mineral oil / 1,2-dimethoxy-ethane / 16 h / Ambient temperature
2: 1.) Hg(ClO4)2*3H2O; 2.) acetic acid / 1.) THF, chloroform, r.t., 15 min; 2.) reflux, 1 h
With
mercury(II) perchlorate; sodium hydride; acetic acid;
In
1,2-dimethoxyethane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 78 percent / sodium hydride / 1,2-dimethoxy-ethane / Ambient temperature
2: 1.) mercuric chloride, 2.) acetic acid / 1.) aqueous MeOH, r.t., 2.) reflux, 1 h
With
sodium hydride; acetic acid; mercury dichloride;
In
1,2-dimethoxyethane;
DOI:10.1246/cl.1987.1199
