(2S,5R,8S,9S,10R,13R,14S,17R)-2-Benzenesulfonylmethyl-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-tetradecahydro-3,4-dioxa-cyclopenta[a]phenanthren-5-ol

Base Information

• Chemical Name: (2S,5R,8S,9S,10R,13R,14S,17R)-2-Benzenesulfonylmethyl-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-tetradecahydro-3,4-dioxa-cyclopenta[a]phenanthren-5-ol
• CAS No.: 211296-33-2
• Molecular Formula: C₃₂H₅₀O₅S
• Molecular Weight: 546.812

Synonyms:(2S,5R,8S,9S,10R,13R,14S,17R)-2-Benzenesulfonylmethyl-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-tetradecahydro-3,4-dioxa-cyclopenta[a]phenanthren-5-ol

Chemical Property of (2S,5R,8S,9S,10R,13R,14S,17R)-2-Benzenesulfonylmethyl-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-tetradecahydro-3,4-dioxa-cyclopenta[a]phenanthren-5-ol

Chemical Property:

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Technology Process of (2S,5R,8S,9S,10R,13R,14S,17R)-2-Benzenesulfonylmethyl-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-tetradecahydro-3,4-dioxa-cyclopenta[a]phenanthren-5-ol

There total 2 articles about (2S,5R,8S,9S,10R,13R,14S,17R)-2-Benzenesulfonylmethyl-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-tetradecahydro-3,4-dioxa-cyclopenta[a]phenanthren-5-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

(2S,5R,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-10,13-dimethyl-2-phenylsulfanylmethyl-tetradecahydro-3,4-dioxa-cyclopenta[a]phenanthren-5-ol (211296-30-9) → (2S,5R,8S,9S,10R,13R,14S,17R)-2-Benzenesulfonylmethyl-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-tetradecahydro-3,4-dioxa-cyclopenta[a]phenanthren-5-ol (211296-33-2)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 1h; Ambient temperature;

DOI:10.1021/jo980319q

Reference yield:

4-nor-3,4-secocholest-2-en-5-one → (2S,5R,8S,9S,10R,13R,14S,17R)-2-Benzenesulfonylmethyl-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-tetradecahydro-3,4-dioxa-cyclopenta[a]phenanthren-5-ol (211296-33-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) O₂, benzenethiol / 1.) acetic acid, rt, 36 h

2: 94 percent / m-CPBA / CH₂Cl₂ / 1 h / Ambient temperature

With oxygen; thiophenol; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

DOI:10.1021/jo980319q

Reference yield:

(2S,5R,8S,9S,10R,13R,14S,17R)-2-Benzenesulfonylmethyl-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-tetradecahydro-3,4-dioxa-cyclopenta[a]phenanthren-5-ol (211296-33-2) → 3-[(1R,3aS,4S,5S,7aR)-5-((3R,5S)-5-Benzenesulfonylmethyl-3-methyl-[1,2]dioxolan-3-yl)-1-((R)-1,5-dimethyl-hexyl)-7a-methyl-octahydro-inden-4-yl]-propionic acid

Guidance literature:

With [bis(acetoxy)iodo]benzene; iodine; In dichloromethane; at 24 - 25 ℃; for 0.5h; Irradiation;

DOI:10.1021/jo980319q

upstream raw materials:

(2S,5R,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-10,13-dimethyl-2-phenylsulfanylmethyl-tetradecahydro-3,4-dioxa-cyclopenta[a]phenanthren-5-ol

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