1-(2-fluorophenyl)ethylphenylsilane

Base Information

• Chemical Name: 1-(2-fluorophenyl)ethylphenylsilane
• CAS No.: 1361129-60-3
• Molecular Formula: C₁₄H₁₅FSi
• Molecular Weight: 230.357
• Mol file: 1361129-60-3.mol

Synonyms:1-(2-fluorophenyl)ethylphenylsilane

Chemical Property of 1-(2-fluorophenyl)ethylphenylsilane

Chemical Property:

Purity/Quality:

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Technology Process of 1-(2-fluorophenyl)ethylphenylsilane

There total 3 articles about 1-(2-fluorophenyl)ethylphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

→ 1-(2-fluorophenyl)ethylphenylsilane (1361129-60-3)

Guidance literature:

With C₄₀H₄₈Cl₂FeN₂; ethylmagnesium bromide; In tetrahydrofuran; at 30 - 35 ℃; for 10h; Glovebox;

Reference yield: 84.0%

2-fluorostyrene (394-46-7) + phenylsilane (694-53-1) → 1-(2-fluorophenyl)ethylphenylsilane (1361129-60-3)

Guidance literature:

With C₁₀H₁₄CoO₅; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; at 20 ℃; for 3h; regioselective reaction;

DOI:10.1021/acscatal.6b02518

Reference yield:

2-fluorostyrene (394-46-7) + phenylsilane (694-53-1) → 1-(2-fluorophenyl)ethylphenylsilane (1361129-60-3) + 1-(2-fluorophenyl)-2-(phenylsilyl)ethane (1361129-61-4)

Guidance literature:

With C₁₇H₁₉N₃Ni⁽¹⁺⁾*C₃₂H₁₂BF₂₄^(1-); In benzene-d6; at 60 ℃; Inert atmosphere;

DOI:10.1021/om200937d

upstream raw materials:

2-fluorostyrene

phenylsilane