3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-(3-methylbutanamido)-3-O-benzyl-4,6-dideoxy-2-O-methyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

Base Information

Chemical Name:3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-(3-methylbutanamido)-3-O-benzyl-4,6-dideoxy-2-O-methyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside
CAS No.:927680-53-3
Molecular Formula:C₇₀H₈₂N₂O₁₇
Molecular Weight:1223.42
Hs Code.:

3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-(3-methylbutanamido)-3-O-benzyl-4,6-dideoxy-2-O-methyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

Synonyms:3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-(3-methylbutanamido)-3-O-benzyl-4,6-dideoxy-2-O-methyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

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Chemical Property of 3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-(3-methylbutanamido)-3-O-benzyl-4,6-dideoxy-2-O-methyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

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Technology Process of 3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-(3-methylbutanamido)-3-O-benzyl-4,6-dideoxy-2-O-methyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

There total 18 articles about 3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-(3-methylbutanamido)-3-O-benzyl-4,6-dideoxy-2-O-methyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 503-74-2
3-methylbutyric acid

: C₆₅H₇₄N₂O₁₆

: 927680-53-3
3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-(3-methylbutanamido)-3-O-benzyl-4,6-dideoxy-2-O-methyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

: C₇₀H₈₂N₂O₁₇

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; for 1h;

Reference yield: 61.0%

: C₆₅H₇₄N₂O₁₆

: 503-74-2
3-methylbutyric acid

: 3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-(3-methylbutanamido)-3-O-benzyl-4,6-dideoxy-2-O-methyl-α-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

: 927680-53-3
3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-(3-methylbutanamido)-3-O-benzyl-4,6-dideoxy-2-O-methyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃; for 4h;
DOI:10.1002/chem.200601245

Reference yield:

: 142776-67-8
ethyl 2-O-benzoyl-4-O-benzyl-1-thio-α-L-rhamnopyranoside

: 927680-53-3
3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-(3-methylbutanamido)-3-O-benzyl-4,6-dideoxy-2-O-methyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 8 steps

1: 72 percent / 4 Angstroem molecular sieves; N-iodosuccinimide; trifluoromethaneulfonic acid / CH₂Cl₂ / 0 °C

2: 78 percent / 4 Angstroem molecular sieves; N-iodosuccinimide; trifluoromethaneulfonic acid / CH₂Cl₂ / 0 °C

3: 93 percent / hyrazine acetate / methanol; CH₂Cl₂ / 4 h / 20 °C

4: 76 percent / 4 Angstroem molecular sieves; N-iodosuccinimide; trifluoromethaneulfonic acid / CH₂Cl₂ / 0 °C

5: 93 percent / hyrazine acetate / methanol; CH₂Cl₂ / 4 h / 20 °C

6: 51 percent / silver(I) oxide / dimethyl sulfide / tetrahydrofuran / 20 °C

7: 99 percent / 1,3-propanedithiol; triethylamine; pyridine / H₂O / 20 °C

8: 61 percent / HATU; 1-hydroxy-7-azabenzotriazole; diisopropylethylamine / dimethylformamide / 4 h / 20 °C

With pyridine; 1.3-propanedithiol; N-iodo-succinimide; 1-hydroxy-7-aza-benzotriazole; trifluorormethanesulfonic acid; 4 A molecular sieve; hydrazinium monoacetate; triethylamine; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; silver(l) oxide; dimethylsulfide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.200601245