sodium 7β--2-phenylacetamido>-7α-formamido-cephalosporanate

Base Information

Chemical Name:sodium 7β--2-phenylacetamido>-7α-formamido-cephalosporanate
CAS No.:86062-39-7
Molecular Formula:C₂₆H₂₇N₆O₁₀S*Na
Molecular Weight:638.59
Hs Code.:

sodium 7β-<D-2-<(4-ethyl-2,3-dioxopiperazin-1-yl)carbonylamino>-2-phenylacetamido>-7α-formamido-cephalosporanate

Synonyms:sodium 7β--2-phenylacetamido>-7α-formamido-cephalosporanate

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Chemical Property of sodium 7β--2-phenylacetamido>-7α-formamido-cephalosporanate

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Technology Process of sodium 7β--2-phenylacetamido>-7α-formamido-cephalosporanate

There total 5 articles about sodium 7β--2-phenylacetamido>-7α-formamido-cephalosporanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 86062-38-6
t-butyl 7β--2-phenylacetamido>-7α-formamidocephalosporanate

: 86062-39-7
sodium 7β--2-phenylacetamido>-7α-formamido-cephalosporanate

Guidance literature:: With formic acid; sodium hydrogencarbonate; In water;

Reference yield:

: 63422-71-9
(R)-α-[[(4-ethyl-2,3-dioxo-1-piperazinyl)carbonyl]amino]benzeneacetic acid

: 86062-39-7
sodium 7β--2-phenylacetamido>-7α-formamido-cephalosporanate

Guidance literature:: Multi-step reaction with 5 steps

1: oxalyl dichloride / CH₂Cl₂ / 1 h / Ambient temperature

2: pyridine / CH₂Cl₂ / 2 h / Ambient temperature

3: 41 percent / mercury(II) acetate, ammonia / dimethylformamide / -40 degC then allowed to warm to room temperature

4: 37 percent / pyridine / CH₂Cl₂

5: 32 percent / formic acid, sodium hydrogen carbonate / H₂O

With pyridine; formic acid; oxalyl dichloride; mercury(II) diacetate; ammonia; sodium hydrogencarbonate; In dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 86062-37-5
t-butyl 7α-amino-7β--2-phenylacetamido>cephalosporanate

: 86062-39-7
sodium 7β--2-phenylacetamido>-7α-formamido-cephalosporanate

Guidance literature:: Multi-step reaction with 2 steps

1: 37 percent / pyridine / CH₂Cl₂

2: 32 percent / formic acid, sodium hydrogen carbonate / H₂O

With pyridine; formic acid; sodium hydrogencarbonate; In dichloromethane; water;