1,6-anhydro-4-O-benzyl-2-deoxy-2-isothiocyanato-3-O-p-toluenesulfonyl-β-D-glucopyranose

Base Information

Chemical Name:1,6-anhydro-4-O-benzyl-2-deoxy-2-isothiocyanato-3-O-p-toluenesulfonyl-β-D-glucopyranose
CAS No.:101024-14-0
Molecular Formula:C₂₁H₂₁NO₆S₂
Molecular Weight:447.533
Hs Code.:

Synonyms:1,6-anhydro-4-O-benzyl-2-deoxy-2-isothiocyanato-3-O-p-toluenesulfonyl-β-D-glucopyranose

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Chemical Property of 1,6-anhydro-4-O-benzyl-2-deoxy-2-isothiocyanato-3-O-p-toluenesulfonyl-β-D-glucopyranose

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Technology Process of 1,6-anhydro-4-O-benzyl-2-deoxy-2-isothiocyanato-3-O-p-toluenesulfonyl-β-D-glucopyranose

There total 3 articles about 1,6-anhydro-4-O-benzyl-2-deoxy-2-isothiocyanato-3-O-p-toluenesulfonyl-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 101024-11-7
1,6-anhydro-4-O-benzyl-2-deoxy-2-isothiocyanato-β-D-glucopyranose

: 98-59-9
p-toluenesulfonyl chloride

: 101024-14-0
1,6-anhydro-4-O-benzyl-2-deoxy-2-isothiocyanato-3-O-p-toluenesulfonyl-β-D-glucopyranose

Guidance literature:: With pyridine; for 4h; Heating;

Reference yield:

: 50447-92-2
2-amino-1,6-anhydro-4-O-benzyl-2-deoxy-β-D-glucopyranose

: 101024-14-0
1,6-anhydro-4-O-benzyl-2-deoxy-2-isothiocyanato-3-O-p-toluenesulfonyl-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogen carbonate / dioxane; H₂O

2: NaOH, I₂ / dioxane; aq. ethanol

3: 77 percent / pyridine / 4 h / Heating

With pyridine; sodium hydroxide; iodine; sodium hydrogencarbonate; In 1,4-dioxane; ethanol; water;

Reference yield:

: 101024-10-6
C₁₄H₁₆NO₄S₂^(1-)*Na⁽¹⁺⁾

: 101024-14-0
1,6-anhydro-4-O-benzyl-2-deoxy-2-isothiocyanato-3-O-p-toluenesulfonyl-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: NaOH, I₂ / dioxane; aq. ethanol

2: 77 percent / pyridine / 4 h / Heating

With pyridine; sodium hydroxide; iodine; In 1,4-dioxane; ethanol;