C₅₆H₇₁N₉O₁₄S

Base Information

Chemical Name:C₅₆H₇₁N₉O₁₄S
CAS No.:1389332-49-3
Molecular Formula:C₅₆H₇₁N₉O₁₄S
Molecular Weight:1126.3
Hs Code.:

C<sub>56</sub>H<sub>71</sub>N<sub>9</sub>O<sub>14</sub>S

Synonyms:C₅₆H₇₁N₉O₁₄S

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Chemical Property of C₅₆H₇₁N₉O₁₄S

Chemical Property:

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Technology Process of C₅₆H₇₁N₉O₁₄S

There total 9 articles about C₅₆H₇₁N₉O₁₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂HF₃O₂*C₄₀H₅₂N₈O₉S

: 5545-52-8
Z-D(tBu)-OH

: 1389332-49-3
C₅₆H₇₁N₉O₁₄S

Guidance literature:: Z-D(tBu)-OH; With 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h; Inert atmosphere;

C₂HF₃O₂*C₄₀H₅₂N₈O₉S; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/chem.201200457

Reference yield:

: C₂HF₃O₂*C₁₇H₂₄N₂O₆

: 1389332-49-3
C₅₆H₇₁N₉O₁₄S

Guidance literature:: Multi-step reaction with 8 steps

1.1: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 18 h / 20 °C / Inert atmosphere

2.1: hydrogen azide; di-isopropyl azodicarboxylate; triphenylphosphine / dichloromethane; N,N-dimethyl-formamide; toluene / 2 h / -20 °C / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 3 h / Inert atmosphere

4.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 18 h / 0 - 20 °C / Inert atmosphere

5.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran / 0.12 h / 0 - 20 °C / Inert atmosphere

6.1: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

6.2: 0 - 20 °C / Inert atmosphere

7.1: dichloromethane / 2 h / 20 °C / Inert atmosphere

8.1: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

8.2: 0 - 20 °C / Inert atmosphere

With hydrogen azide; 1-hydroxy-7-aza-benzotriazole; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; N-ethyl-N,N-diisopropylamine; triphenylphosphine; HATU; lithium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol; toluene;
DOI:10.1002/chem.201200457

Reference yield:

: 1389331-98-9
C₂₂H₃₂N₂O₈

: 1389332-49-3
C₅₆H₇₁N₉O₁₄S

Guidance literature:: Multi-step reaction with 9 steps

1.1: dichloromethane / 2 h / 20 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 18 h / 20 °C / Inert atmosphere

3.1: hydrogen azide; di-isopropyl azodicarboxylate; triphenylphosphine / dichloromethane; N,N-dimethyl-formamide; toluene / 2 h / -20 °C / Inert atmosphere

4.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 3 h / Inert atmosphere

5.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 18 h / 0 - 20 °C / Inert atmosphere

6.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran / 0.12 h / 0 - 20 °C / Inert atmosphere

7.1: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

7.2: 0 - 20 °C / Inert atmosphere

8.1: dichloromethane / 2 h / 20 °C / Inert atmosphere

9.1: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

9.2: 0 - 20 °C / Inert atmosphere

With hydrogen azide; 1-hydroxy-7-aza-benzotriazole; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; N-ethyl-N,N-diisopropylamine; triphenylphosphine; HATU; lithium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol; toluene;
DOI:10.1002/chem.201200457