AG-690/15438099

Base Information

Chemical Name:AG-690/15438099
CAS No.:397281-20-8
Molecular Formula:C₁₇H₁₁ClN₂O₄S
Molecular Weight:374.804
Hs Code.:
Mol file:397281-20-8.mol

Synonyms:AG-690/15438099

Suppliers and Price of AG-690/15438099

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of AG-690/15438099

Chemical Property:

PKA:8.04±0.31(Predicted)
Density:1.651±0.06 g/cm3(Predicted)

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of AG-690/15438099

There total 6 articles about AG-690/15438099 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 3964-52-1
2-chloro 4-aminophenol

: 78078-92-9
2-oxo-1,2-dihydrobenzo[cd]indole-6-sulfonyl chloride

: 397281-20-8
AG-690/15438099

Guidance literature:: With pyridine; In tetrahydrofuran; at 20 ℃; for 20h;
DOI:10.3109/14756366.2014.895718

Reference yield:

: 7797-81-1
N-hydroxy-1,8-naphthalenedicarboximide

: 397281-20-8
AG-690/15438099

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / ethanol; water / 3 h / Reflux

2.1: nitric acid; acetic acid / 1 h / 50 °C

3.1: palladium 10% on activated carbon; hydrogen / ethanol

4.1: hydrogenchloride / water / 0.5 h / 40 °C

4.2: 0.5 h / 0 °C

4.3: 1 h

5.1: pyridine / tetrahydrofuran / 20 h / 20 °C

With pyridine; hydrogenchloride; palladium 10% on activated carbon; hydrogen; nitric acid; acetic acid; sodium hydroxide; In tetrahydrofuran; ethanol; water;
DOI:10.3109/14756366.2014.895718

Reference yield:

: 81-84-5
1,8-Naphthalic anhydride

: 397281-20-8
AG-690/15438099

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydroxylamine hydrochloride; pyridine / 1 h / 80 °C / Reflux

1.2: 1 h / Reflux

2.1: sodium hydroxide / ethanol; water / 3 h / Reflux

3.1: nitric acid; acetic acid / 1 h / 50 °C

4.1: palladium 10% on activated carbon; hydrogen / ethanol

5.1: hydrogenchloride / water / 0.5 h / 40 °C

5.2: 0.5 h / 0 °C

5.3: 1 h

6.1: pyridine / tetrahydrofuran / 20 h / 20 °C

With pyridine; hydrogenchloride; palladium 10% on activated carbon; hydroxylamine hydrochloride; hydrogen; nitric acid; acetic acid; sodium hydroxide; In tetrahydrofuran; ethanol; water;
DOI:10.3109/14756366.2014.895718