Technology Process of C38H28F3N7
There total 13 articles about C38H28F3N7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
di-isopropyl azodicarboxylate; diphenyl phosphoryl azide; triphenylphosphine;
at 0 - 20 ℃;
for 16h;
DOI:10.1016/j.bmcl.2014.05.082
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydroxide / tetrahydrofuran; methanol / 1 h / 0 °C
2: diphenyl phosphoryl azide; triphenylphosphine; di-isopropyl azodicarboxylate / 16 h / 0 - 20 °C
With
di-isopropyl azodicarboxylate; diphenyl phosphoryl azide; triphenylphosphine; sodium hydroxide;
In
tetrahydrofuran; methanol;
DOI:10.1016/j.bmcl.2014.05.082
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: palladium diacetate; 1,4-di(diphenylphosphino)-butane; tert-butylamine; propyl cyanide / water / 16 h / 120 °C
2.1: bis(tri-t-butylphosphine)palladium(0); N-ethyl-N,N-diisopropylamine / 1,4-dioxane / 0.5 h / 130 °C / Microwave irradiation
2.2: 5 h / 20 °C / 760.05 Torr
3.1: sodium hydroxide / tetrahydrofuran; methanol / 1 h / 0 °C
4.1: diphenyl phosphoryl azide; triphenylphosphine; di-isopropyl azodicarboxylate / 16 h / 0 - 20 °C
With
propyl cyanide; bis(tri-t-butylphosphine)palladium(0); di-isopropyl azodicarboxylate; diphenyl phosphoryl azide; palladium diacetate; tert-butylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; 1,4-di(diphenylphosphino)-butane; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; methanol; water;
1.1: |Suzuki Coupling / 2.1: |Heck Reaction;
DOI:10.1016/j.bmcl.2014.05.082
