2,6-dimethoxy-4-(methoxymethyl)phenyl triflate

Base Information

Chemical Name:2,6-dimethoxy-4-(methoxymethyl)phenyl triflate
CAS No.:124200-73-3
Molecular Formula:C₁₁H₁₃F₃O₆S
Molecular Weight:330.282
Hs Code.:

Synonyms:2,6-dimethoxy-4-(methoxymethyl)phenyl triflate

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Chemical Property of 2,6-dimethoxy-4-(methoxymethyl)phenyl triflate

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Technology Process of 2,6-dimethoxy-4-(methoxymethyl)phenyl triflate

There total 1 articles about 2,6-dimethoxy-4-(methoxymethyl)phenyl triflate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 60824-64-8
4-hydroxy-3,5-dimethoxybenzyl methyl ether

: 124200-73-3
2,6-dimethoxy-4-(methoxymethyl)phenyl triflate

Guidance literature:: With 2,4,6-trimethyl-pyridine; In dichloromethane; at 0 ℃;
DOI:10.1021/jo00290a033

Reference yield: 81.0%

: 124200-73-3
2,6-dimethoxy-4-(methoxymethyl)phenyl triflate

: 73569-69-4
1-methylmethoxy-3,5-dimethoxybenzene

Guidance literature:: With hydrogen; triethylamine; palladium on activated charcoal; In methanol; under 3361.5 Torr; other reagents, other solvent, other temp., other catalysts;
DOI:10.1021/jo00290a033

Reference yield:

: 124200-73-3
2,6-dimethoxy-4-(methoxymethyl)phenyl triflate

: 4179-19-5
1,3-dimethoxy-5-methylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / H₂, triethylamine / 10percent Pd/C / methanol / 3361.5 Torr / other reagents, other solvent, other temp., other catalysts

2: 98 percent / H₂ / 10percent Pd/C / methanol / 0.5 h / 1706.6 Torr

With hydrogen; triethylamine; palladium on activated charcoal; In methanol;
DOI:10.1021/jo00290a033