erythro-3-<3'',4''-dimethoxy-α,α-bis(phenylthio)benzyl>-2-(α-hydroxy-3',4'-methylenedioxybenzyl)-γ-butyrolactone

Base Information

Chemical Name:erythro-3-<3'',4''-dimethoxy-α,α-bis(phenylthio)benzyl>-2-(α-hydroxy-3',4'-methylenedioxybenzyl)-γ-butyrolactone
CAS No.:103844-12-8
Molecular Formula:C₃₃H₃₀O₇S₂
Molecular Weight:602.729
Hs Code.:

Synonyms:erythro-3-<3'',4''-dimethoxy-α,α-bis(phenylthio)benzyl>-2-(α-hydroxy-3',4'-methylenedioxybenzyl)-γ-butyrolactone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of erythro-3-<3'',4''-dimethoxy-α,α-bis(phenylthio)benzyl>-2-(α-hydroxy-3',4'-methylenedioxybenzyl)-γ-butyrolactone

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of erythro-3-<3'',4''-dimethoxy-α,α-bis(phenylthio)benzyl>-2-(α-hydroxy-3',4'-methylenedioxybenzyl)-γ-butyrolactone

There total 3 articles about erythro-3-<3'',4''-dimethoxy-α,α-bis(phenylthio)benzyl>-2-(α-hydroxy-3',4'-methylenedioxybenzyl)-γ-butyrolactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 103844-12-8
erythro-3-<3'',4''-dimethoxy-α,α-bis(phenylthio)benzyl>-2-(α-hydroxy-3',4'-methylenedioxybenzyl)-γ-butyrolactone

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / HCl gas / CHCl₃ / 1 h / 0 °C

2: 1.) BuLi / 1.) THF, - 78 deg C, 30 min; 2.) THF, -78 deg C, 90 min; 3.) THF, -78 deg C, 2 h

With hydrogenchloride; n-butyllithium; In chloroform;

Reference yield:

: 108-98-5
thiophenol

: 103844-12-8
erythro-3-<3'',4''-dimethoxy-α,α-bis(phenylthio)benzyl>-2-(α-hydroxy-3',4'-methylenedioxybenzyl)-γ-butyrolactone

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / HCl gas / CHCl₃ / 1 h / 0 °C

2: 1.) BuLi / 1.) THF, - 78 deg C, 30 min; 2.) THF, -78 deg C, 90 min; 3.) THF, -78 deg C, 2 h

With hydrogenchloride; n-butyllithium; In chloroform;