ethyl N-(2-{4-[2-({[(tert-butoxycarbonyl)amino][(tert-butoxycarbonyl)imino]methyl}amino)ethyl]-1H-1,2,3-triazol-1-yl}ethyl)-N-[(4-methylphenyl)sulfonyl]glycinate

Base Information

Chemical Name:ethyl N-(2-{4-[2-({[(tert-butoxycarbonyl)amino][(tert-butoxycarbonyl)imino]methyl}amino)ethyl]-1H-1,2,3-triazol-1-yl}ethyl)-N-[(4-methylphenyl)sulfonyl]glycinate
CAS No.:1325689-00-6
Molecular Formula:C₂₈H₄₃N₇O₈S
Molecular Weight:637.758
Hs Code.:

ethyl N-(2-{4-[2-({[(tert-butoxycarbonyl)amino][(tert-butoxycarbonyl)imino]methyl}amino)ethyl]-1H-1,2,3-triazol-1-yl}ethyl)-N-[(4-methylphenyl)sulfonyl]glycinate

Synonyms:ethyl N-(2-{4-[2-({[(tert-butoxycarbonyl)amino][(tert-butoxycarbonyl)imino]methyl}amino)ethyl]-1H-1,2,3-triazol-1-yl}ethyl)-N-[(4-methylphenyl)sulfonyl]glycinate

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Chemical Property of ethyl N-(2-{4-[2-({[(tert-butoxycarbonyl)amino][(tert-butoxycarbonyl)imino]methyl}amino)ethyl]-1H-1,2,3-triazol-1-yl}ethyl)-N-[(4-methylphenyl)sulfonyl]glycinate

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Technology Process of ethyl N-(2-{4-[2-({[(tert-butoxycarbonyl)amino][(tert-butoxycarbonyl)imino]methyl}amino)ethyl]-1H-1,2,3-triazol-1-yl}ethyl)-N-[(4-methylphenyl)sulfonyl]glycinate

There total 4 articles about ethyl N-(2-{4-[2-({[(tert-butoxycarbonyl)amino][(tert-butoxycarbonyl)imino]methyl}amino)ethyl]-1H-1,2,3-triazol-1-yl}ethyl)-N-[(4-methylphenyl)sulfonyl]glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1243153-82-3
N,N'-di-Boc-N''-(but-3-ynyl)-guanidine

: 1325688-62-7
[(2-azido-ethyl)-(toluene-4-sulfonyl)amino]acetic acid ethyl ester

: 1325689-00-6
ethyl N-(2-{4-[2-({[(tert-butoxycarbonyl)amino][(tert-butoxycarbonyl)imino]methyl}amino)ethyl]-1H-1,2,3-triazol-1-yl}ethyl)-N-[(4-methylphenyl)sulfonyl]glycinate

Guidance literature:: With copper(I) iodide triethylphosphite; In tetrahydrofuran; at 80 ℃; for 0.416667h; Inert atmosphere; Microwave irradiation;

Reference yield:

: 214709-53-2
(2-hydroxy-ethylamino)-acetic acid ethyl ester

: 1325689-00-6
ethyl N-(2-{4-[2-({[(tert-butoxycarbonyl)amino][(tert-butoxycarbonyl)imino]methyl}amino)ethyl]-1H-1,2,3-triazol-1-yl}ethyl)-N-[(4-methylphenyl)sulfonyl]glycinate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 4 h / 0 °C

2: triphenylphosphine; di-isopropyl azodicarboxylate; diphenyl phosphoryl azide / tetrahydrofuran / 2 h / -10 - 20 °C

3: copper(I) iodide triethylphosphite / tetrahydrofuran / 0.42 h / 80 °C / Inert atmosphere; Microwave irradiation

With di-isopropyl azodicarboxylate; copper(I) iodide triethylphosphite; diphenyl phosphoryl azide; triethylamine; triphenylphosphine; In tetrahydrofuran;

Reference yield:

: 1325688-65-0
ethyl N-(2-hydroxyethyl)-N-[(4-methylphenyl)sulfonyl]glycinate

: 1325689-00-6
ethyl N-(2-{4-[2-({[(tert-butoxycarbonyl)amino][(tert-butoxycarbonyl)imino]methyl}amino)ethyl]-1H-1,2,3-triazol-1-yl}ethyl)-N-[(4-methylphenyl)sulfonyl]glycinate

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate; diphenyl phosphoryl azide / tetrahydrofuran / 2 h / -10 - 20 °C

2: copper(I) iodide triethylphosphite / tetrahydrofuran / 0.42 h / 80 °C / Inert atmosphere; Microwave irradiation

With di-isopropyl azodicarboxylate; copper(I) iodide triethylphosphite; diphenyl phosphoryl azide; triphenylphosphine; In tetrahydrofuran;