N-(5-(2-(4-(4-(4-aminobutyl)phenyl)-1(S)-methylbutylamino)-1(R)-hydroxyethyl)-2-hydroxyphenyl)formamide

Base Information

Chemical Name:N-(5-(2-(4-(4-(4-aminobutyl)phenyl)-1(S)-methylbutylamino)-1(R)-hydroxyethyl)-2-hydroxyphenyl)formamide
CAS No.:960398-22-5
Molecular Formula:C₂₄H₃₅N₃O₃
Molecular Weight:413.56
Hs Code.:

Synonyms:N-(5-(2-(4-(4-(4-aminobutyl)phenyl)-1(S)-methylbutylamino)-1(R)-hydroxyethyl)-2-hydroxyphenyl)formamide

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Chemical Property of N-(5-(2-(4-(4-(4-aminobutyl)phenyl)-1(S)-methylbutylamino)-1(R)-hydroxyethyl)-2-hydroxyphenyl)formamide

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Technology Process of N-(5-(2-(4-(4-(4-aminobutyl)phenyl)-1(S)-methylbutylamino)-1(R)-hydroxyethyl)-2-hydroxyphenyl)formamide

There total 4 articles about N-(5-(2-(4-(4-(4-aminobutyl)phenyl)-1(S)-methylbutylamino)-1(R)-hydroxyethyl)-2-hydroxyphenyl)formamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 960398-21-4
(4-(4-(4-(2-(4-benzyloxy-3-formylaminophenyl)-2(R)-hydroxyethylamino)pentyl)phenyl)butyl)carbamic acid benzyl ester

: 960398-23-6
N-(5-(2-(4-(4-(4-aminobutyl)phenyl)-1(R)-methylbutylamino)-1(R)-hydroxyethyl)-2-hydroxyphenyl)formamide

: 960398-22-5
N-(5-(2-(4-(4-(4-aminobutyl)phenyl)-1(S)-methylbutylamino)-1(R)-hydroxyethyl)-2-hydroxyphenyl)formamide

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In methanol; ethanol; at 20 ℃; for 4h; under 760.051 Torr;

Reference yield:

: 960398-19-0
(4-(4-(4-(1,3-dioxo-1,3-dihydroisoindol-2-yl)pentyl)phenyl)butyl)carbamic acid benzyl ester

: 960398-23-6
N-(5-(2-(4-(4-(4-aminobutyl)phenyl)-1(R)-methylbutylamino)-1(R)-hydroxyethyl)-2-hydroxyphenyl)formamide

: 960398-22-5
N-(5-(2-(4-(4-(4-aminobutyl)phenyl)-1(S)-methylbutylamino)-1(R)-hydroxyethyl)-2-hydroxyphenyl)formamide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine / ethanol / 3 h / 75 °C

2: potassium carbonate / chloroform / 72 h / Heating / reflux

3: hydrogen / palladium 10% on activated carbon / methanol; ethanol / 4 h / 20 °C / 760.05 Torr

With hydrogen; potassium carbonate; hydrazine; palladium 10% on activated carbon; In methanol; ethanol; chloroform;

Reference yield:

: 201677-59-0
N-[5-((1R)-2-bromo-1-hydroxyethyl)-2-(phenylmethoxy)phenyl]carboxamide

: 960398-23-6
N-(5-(2-(4-(4-(4-aminobutyl)phenyl)-1(R)-methylbutylamino)-1(R)-hydroxyethyl)-2-hydroxyphenyl)formamide

: 960398-22-5
N-(5-(2-(4-(4-(4-aminobutyl)phenyl)-1(S)-methylbutylamino)-1(R)-hydroxyethyl)-2-hydroxyphenyl)formamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / chloroform / 72 h / Heating / reflux

2: hydrogen / palladium 10% on activated carbon / methanol; ethanol / 4 h / 20 °C / 760.05 Torr

With hydrogen; potassium carbonate; palladium 10% on activated carbon; In methanol; ethanol; chloroform;