(dppe)Pd(5-nitrodopamine^(2-))

Base Information

Chemical Name:(dppe)Pd(5-nitrodopamine^(2-))
CAS No.:868962-05-4
Molecular Formula:C₃₄H₃₂N₂O₄P₂Pd
Molecular Weight:701.007
Hs Code.:

(dppe)Pd(5-nitrodopamine<sup>(2-)</sup>)

Synonyms:(dppe)Pd(5-nitrodopamine^(2-))

Suppliers and Price of (dppe)Pd(5-nitrodopamine^(2-))

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (dppe)Pd(5-nitrodopamine^(2-))

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Technology Process of (dppe)Pd(5-nitrodopamine^(2-))

There total 1 articles about (dppe)Pd(5-nitrodopamine^(2-)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 19978-61-1
(1,2-bis(diphenylphosphanyl)ethane)dichloridopalladium(II)

: 21581-49-7
4-(2-aminoethyl)-5-nitrobenzene-1,2-diol

: 868962-05-4
(dppe)Pd(5-nitrodopamine^(2-))

Guidance literature:: With NaBF₄; KOH; In dichloromethane; water; under N2 atm. to suspn. NaBF4 and (dppe)PdCl2 in CH2Cl2 aq. soln. 5-nitrodopamine and KOH was added and stirred for 1 h; CH2Cl2 was added, organic layer was dried over MgSO4, filtered, and concd., MeOH was added, solvent was removed in vacuo, residue was dried in vacuo; elem. anal.;
DOI:10.1021/om050639h

Reference yield: 93.0%

: tetrafluoroboric acid

: 17455-13-9
18-crown-6 ether

: 868962-05-4
(dppe)Pd(5-nitrodopamine^(2-))

: 868962-06-5
(((C₆H₅)2PCH₂)2)Pd(O₂C₆H₂(NO₂)CH₂CH₂NH₃)⁽¹⁺⁾*BF₄^(1-)*O₆C₁₂H₂₄=((((C₆H₅)2PCH₂)2)Pd(O₂C₆H₂(NO₂)CH₂CH₂NH₃))BF₄*O₆C₁₂H₂₄

Guidance literature:: In diethyl ether; dichloromethane; under N2 atm. to soln. Pd complex and 18-crown-6 in CH2Cl2 54% soln. HBF4 in Et2O was added and stirred for 5 min; Et2O was added, ppt. was filtered, washed with Et2O; elem. anal.;
DOI:10.1021/om050639h