16-CARBOXYHEXADECYL DISULFIDE, 99%

Base Information

• Chemical Name: 16-CARBOXYHEXADECYL DISULFIDE, 99%
• CAS No.: 112122-99-3
• Molecular Formula: C32H62 O4 S2
• Molecular Weight: 603.01544
• Mol file: 112122-99-3.mol

Synonyms:16-CARBOXYHEXADECYL DISULFIDE, 99%

Chemical Property of 16-CARBOXYHEXADECYL DISULFIDE, 99%

Chemical Property:

• PSA: 125.20000
• LogP: 12.24000
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 16-CARBOXYHEXADECYL DISULFIDE, 99%

There total 4 articles about 16-CARBOXYHEXADECYL DISULFIDE, 99% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

16-mercaptohexadecanoic acid (69839-68-5) → 16,16'-dithiobis(hexadecanoic acid) (112122-99-3)

Guidance literature:

With potassium triiodide; In chloroform;

DOI:10.1021/ja058701p

Reference yield:

C16H31O5S2(1-)*Na(1+) → 16,16'-dithiobis(hexadecanoic acid) (112122-99-3)

Guidance literature:

With hydrogenchloride; thiourea; In ethanol; Yield given; Heating;

DOI:10.1039/cc9960001193

Reference yield:

16-hydroxyhexadecanoic acid (506-13-8) → 16,16'-dithiobis(hexadecanoic acid) (112122-99-3)

Guidance literature:

Multi-step reaction with 3 steps

1: NEt₃ / tetrahydrofuran / 0 °C / Heating

2: Na₂S₂O₃ / aq. ethanol / Heating

3: thiourea, aq. HCl / ethanol / Heating

With hydrogenchloride; sodium thiosulfate; triethylamine; thiourea; In tetrahydrofuran; ethanol;

DOI:10.1039/cc9960001193

upstream raw materials:

16-mercaptohexadecanoic acid

16-hydroxyhexadecanoic acid

16-<(methylsulfonyl)oxy>hexadecanoic acid