2-{3-[(tert-butoxycarbonyl)amino]-2-methoxypyridin-4-yl}ethyl methanesulfonate

Base Information

Chemical Name:2-{3-[(tert-butoxycarbonyl)amino]-2-methoxypyridin-4-yl}ethyl methanesulfonate
CAS No.:1338219-72-9
Molecular Formula:C₁₄H₂₂N₂O₆S
Molecular Weight:346.404
Hs Code.:

Synonyms:2-{3-[(tert-butoxycarbonyl)amino]-2-methoxypyridin-4-yl}ethyl methanesulfonate

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Chemical Property of 2-{3-[(tert-butoxycarbonyl)amino]-2-methoxypyridin-4-yl}ethyl methanesulfonate

Chemical Property:

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Technology Process of 2-{3-[(tert-butoxycarbonyl)amino]-2-methoxypyridin-4-yl}ethyl methanesulfonate

There total 1 articles about 2-{3-[(tert-butoxycarbonyl)amino]-2-methoxypyridin-4-yl}ethyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20265-38-7
3-amino-2-methoxypyridine

: 1338219-72-9
2-{3-[(tert-butoxycarbonyl)amino]-2-methoxypyridin-4-yl}ethyl methanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,4-dioxane / 4 h / Reflux

2.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / diethyl ether; hexane / -78 - -15 °C

2.2: -70 - 20 °C

2.3: 0 °C

3.1: triethylamine / dichloromethane / 0 - 20 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; triethylamine; In 1,4-dioxane; diethyl ether; hexane; dichloromethane;
DOI:10.1016/j.tetlet.2011.08.009

Reference yield:

: 1338219-72-9
2-{3-[(tert-butoxycarbonyl)amino]-2-methoxypyridin-4-yl}ethyl methanesulfonate

: 1338219-67-2
2,3-dihydro-1H-pyrrolo[2,3-c]pyridin-7-yl(phenyl)methanone

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 - 20 °C

2.1: sodium thiomethoxide / N,N-dimethyl-formamide / 16 h / 100 °C / Inert atmosphere

3.1: trichlorophosphate / N,N-dimethyl-formamide; toluene / 7 h / 90 °C

4.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,1'-bis-(diphenylphosphino)ferrocene / N,N-dimethyl-formamide / 130 °C

5.1: tetrahydrofuran / -5 - 20 °C

5.2: pH 1

With 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; lithium hexamethyldisilazane; trichlorophosphate; sodium thiomethoxide; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tetlet.2011.08.009

Reference yield:

: 1338219-72-9
2-{3-[(tert-butoxycarbonyl)amino]-2-methoxypyridin-4-yl}ethyl methanesulfonate

: 1338219-65-0
7-chloro-2,3-dihydro-1H-pyrrolo[2,3-c]pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: lithium hexamethyldisilazane / tetrahydrofuran / -78 - 20 °C

2: sodium thiomethoxide / N,N-dimethyl-formamide / 16 h / 100 °C / Inert atmosphere

3: trichlorophosphate / N,N-dimethyl-formamide; toluene / 7 h / 90 °C

With lithium hexamethyldisilazane; trichlorophosphate; sodium thiomethoxide; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tetlet.2011.08.009