3-<(Z,Z)-pentadeca-8,11-dienyl>anisole

Base Information

Chemical Name:3-<(Z,Z)-pentadeca-8,11-dienyl>anisole
CAS No.:51110-46-4
Molecular Formula:C₂₂H₃₄O
Molecular Weight:314.511
Hs Code.:

Synonyms:3-<(Z,Z)-pentadeca-8,11-dienyl>anisole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-<(Z,Z)-pentadeca-8,11-dienyl>anisole

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Technology Process of 3-<(Z,Z)-pentadeca-8,11-dienyl>anisole

There total 33 articles about 3-<(Z,Z)-pentadeca-8,11-dienyl>anisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 51110-45-3
3-(pentadeca-8,11-diynyl)anisole

: 51110-46-4
3-<(Z,Z)-pentadeca-8,11-dienyl>anisole

Guidance literature:: With quinoline; hydrogen; palladium on barium sulfate; In ethyl acetate; Ambient temperature;

Reference yield:

: 2009-84-9
(chloro-6' hexyloxy)-2 tetrahydropyranne

: 51110-46-4
3-<(Z,Z)-pentadeca-8,11-dienyl>anisole

Guidance literature:: Multi-step reaction with 10 steps

1: 1.) Mg / 1.) THF, 2.) THF, 24 h

2: 81 percent / toluene-4-sulphonic acid / ethanol / 24 h / Heating

3: 1.) KOH, 2.) H₂, H₂SO₄ / 2.) 10percent Pd/C / 1.) ethanol, 1 h, reflux, 2.) ethanol, r.t.

4: 4.31 g / PBr₃ / CHCl₃ / 4 h / 0 °C

5: 1.) LiNH₂, Fe(NO₃)3 / 1.) liq. NH₃, THF, HMPA, 2.) liq. NH₃, THF, HMPA, 40 deg C, 24 h

6: p-TsOH / ethanol / 3 h / Heating

7: 0.1704 g / PBr₃ / CHCl₃ / 16 h / -30 deg C to r. t.

8: 1.) EtMgBr, CuCl / 1.) THF, 1 h, 2.) THF, 72 h, 35 deg C

9: 50 percent / H₂, quinoline / 5 percent Pd-BaSO₄ / ethyl acetate / 2 h / Ambient temperature

10: K₂CO₃ / benzene

With quinoline; potassium hydroxide; lithium amide; sulfuric acid; ethylmagnesium bromide; hydrogen; phosphorus tribromide; potassium carbonate; toluene-4-sulfonic acid; magnesium; ferric nitrate; copper(l) chloride; palladium on activated charcoal; palladium on barium sulfate; In ethanol; chloroform; ethyl acetate; benzene;

Reference yield:

: 629-11-8
1,6-hexanediol

: 51110-46-4
3-<(Z,Z)-pentadeca-8,11-dienyl>anisole

Guidance literature:: Multi-step reaction with 9 steps

1: 66 percent / conc. HCl, CuCl / toluene / 24 h / 100 °C

2: 84 percent / K₂CO₃ / benzene / 24 h / Heating

3: 2.) H₂

4: 64 percent / PBr₃ / benzene / 1.) 1 h, 2.) reflux, 3 h

5: 1.) LiNH₂, Fe(NO₃)3 / 1.) liq. NH₃, THF, HMPA, 20 min, 2.) liq. NH₃, THF, HMPA, 16 h

6: p-TsOH / ethanol / 0.33 h / Heating

7: PBr₃ / CHCl₃ / 16 h

8: 1.) EtMgBr, CuCl / 1.) THF, 1 h, 2.) THF, 16 h, 35 deg C

9: 90 percent / H₂, quinoline / 5 percent Pd-BaSO₄ / ethyl acetate / Ambient temperature

With quinoline; hydrogenchloride; lithium amide; ethylmagnesium bromide; hydrogen; phosphorus tribromide; potassium carbonate; toluene-4-sulfonic acid; ferric nitrate; copper(l) chloride; palladium on barium sulfate; In ethanol; chloroform; ethyl acetate; toluene; benzene;