2-thioxo-2-(1,2-O-isopropylideneglycero)-3-N-benzyl-1,3,2-oxaazaphospholane

Base Information

Chemical Name:2-thioxo-2-(1,2-O-isopropylideneglycero)-3-N-benzyl-1,3,2-oxaazaphospholane
CAS No.:100664-83-3
Molecular Formula:C₁₅H₂₂NO₄PS
Molecular Weight:343.384
Hs Code.:

Synonyms:2-thioxo-2-(1,2-O-isopropylideneglycero)-3-N-benzyl-1,3,2-oxaazaphospholane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-thioxo-2-(1,2-O-isopropylideneglycero)-3-N-benzyl-1,3,2-oxaazaphospholane

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Technology Process of 2-thioxo-2-(1,2-O-isopropylideneglycero)-3-N-benzyl-1,3,2-oxaazaphospholane

There total 3 articles about 2-thioxo-2-(1,2-O-isopropylideneglycero)-3-N-benzyl-1,3,2-oxaazaphospholane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 100664-85-5
2-(1,2-O-isopropylideneglycero)-3-N-benzyl-1,3,2-oxaazaphospholane

: 100664-83-3
2-thioxo-2-(1,2-O-isopropylideneglycero)-3-N-benzyl-1,3,2-oxaazaphospholane

Guidance literature:: With sulfur; In benzene; at 20 ℃; for 2h;

Reference yield:

: 104-63-2
N-Benzylethanolamine

: 100664-83-3
2-thioxo-2-(1,2-O-isopropylideneglycero)-3-N-benzyl-1,3,2-oxaazaphospholane

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / 0.5 h / 70 - 80 °C

2: 83 percent / S / benzene / 2 h / 20 °C

With sulfur; In benzene;

Reference yield:

: 34832-91-2
1,2-O-isopropylideneglyceryl N,N,N'N,-tetraethylphosphorodiamidite

: 100664-83-3
2-thioxo-2-(1,2-O-isopropylideneglycero)-3-N-benzyl-1,3,2-oxaazaphospholane

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / 0.5 h / 70 - 80 °C

2: 83 percent / S / benzene / 2 h / 20 °C

With sulfur; In benzene;